Deep eutectic solvent-based microwave-assisted extraction of genistin, genistein and apigenin from pigeon pea roots

被引：168
作者：
Cui, Qi [1 ,2 ]
Peng, Xiao [1 ,2 ]
Yao, Xiao-Hui [1 ,2 ]
Wei, Zuo-Fu [1 ,2 ]
Luo, Meng [1 ,2 ]
Wang, Wei [1 ,2 ]
Zhao, Chun-Jian [1 ,2 ]
Fu, Yu-Jie [1 ,2 ,3 ]
Zu, Yuan-Gang [1 ,2 ]
机构：
[1] Northeast Forestry Univ, Key Lab Forest Plant Ecol, Minist Educ, Harbin 150040, Peoples R China
[2] Northeast Forestry Univ, Engn Res Ctr Forest Biopreparat, Minist Educ, Harbin 150040, Peoples R China
[3] Northeast Forestry Univ, Collaborat Innovat Ctr Dev & Utilizat Forest Reso, Harbin 150040, Peoples R China
来源：
SEPARATION AND PURIFICATION TECHNOLOGY | 2015年 / 150卷
基金：
中国国家自然科学基金;
关键词：
Deep eutectic solvent; Microwave-assisted extraction; Pigeon pea roots; Kinetics; Response surface methodology; PRESSURE CAVITATION EXTRACTION; FLAVONOIDS; OPTIMIZATION; ACID; DRUG;
D O I：
10.1016/j.seppur.2015.06.026
中图分类号：
TQ [化学工业];
学科分类号：
0817 ;
摘要：
The purpose of the study was to develop a new deep eutectic solvent-based microwave-assisted extraction (DES-MAE) method for extracting the three major active compounds genistin, genistein and apigenin from pigeon pea roots. Optimal conditions for DES-MAE, proposed by the single factor and the Box-Behnken design (BBD) tests, were 30% of water in 1,6-hexanediol/ChCl (7:1, mol/mol) as the extraction solvent, microwave power 600W, liquid/solid ratio 14 mL/g, temperature 80 degrees C and time 11 min. The yields of genistin, genistein and apigenin reached 0.449, 0.617 and 0.221 mg/g DW, respectively. The kinetics experiment showed the prominent advantages of DES-MAE such as higher extraction efficiency than other extraction methods. The present results showed that DES could be a kind of green solvent for fast and efficient extraction of the active ingredients from plant materials. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码：63 / 72
页数：10
相关论文
共 50 条
[31]   Enzyme pretreatment and negative pressure cavitation extraction of genistein and apigenin from the roots of pigeon pea [Cajanus cajan (L.) Millspl and the evaluation of antioxidant activity [J].
Zhang, Dong-Yang ;
Zu, Yuan-Gang ;
Fu, Yu-Jie ;
Luo, Meng ;
Wang, Wei ;
Gu, Cheng-Bo ;
Zhao, Chun-Jian ;
Jiao, Jiao ;
Efferth, Thomas .
INDUSTRIAL CROPS AND PRODUCTS, 2012, 37 (01) :311-320
[32]   Microwave-assisted extraction of bioactive compounds from Urtica dioica using solvent-based process optimization and characterization [J].
Sahal, Anjali ;
Hussain, Afzal ;
Mishra, Ritesh ;
Pandey, Sakshi ;
Dobhal, Ankita ;
Ahmad, Waseem ;
Kumar, Vinod ;
Lohani, Umesh Chandra ;
Kumar, Sanjay .
SCIENTIFIC REPORTS, 2025, 15 (01)
[33]   Microwave-assisted hydrodistillation extraction based on microwave-assisted preparation of deep eutectic solvents coupled with GC-MS for analysis of essential oils from clove buds [J].
Chen, Yao ;
Xu, Fangxiang ;
Pang, Mingmei ;
Jin, Xiangzi ;
Lv, Huihao ;
Li, Zuguang ;
Lee, Mawrong .
SUSTAINABLE CHEMISTRY AND PHARMACY, 2022, 27
[34]   Green extraction of apigenin and luteolin from celery seed using deep eutectic solvent [J].
Nguyen Thu Hang ;
Trieu Thi Tu Uyen ;
Nguyen Van Phuong .
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2022, 207
[35]   Optimization of Deep Eutectic Solvent-Based Ultrasound-Assisted Extraction of Bioactive Compounds from Maca Leaves Using the Taguchi Method [J].
Lee, Eun Ji ;
Yoon, Kyung Young .
MOLECULES, 2025, 30 (07)
[36]   Advancements in deep eutectic solvent-based membranes for the extraction, separation, and preconcentration of organic compounds [J].
Sani, Nur Fitrah Abdullah ;
Ramadhan, Rico ;
Yahaya, Noorfatimah ;
Ghadzi, Siti Maisharah Sheikh ;
Mohamed, Ahmad Husaini ;
Kamaruzaman, Sazlinda ;
Ibrahim, Wan Nazihah Wan ;
Hanapi, Nor Suhaila Mohamad ;
Zain, Nur Nadhirah Mohamad .
ADVANCES IN SAMPLE PREPARATION, 2025, 14
[37]   Microwave-assisted extraction of pectin from orange peel using deep eutectic solvents [J].
Turan, Ozlem ;
Isci, Asli ;
Yilmaz, Merve Silanur ;
Tolun, Aysu ;
Sakiyan, Ozge .
SUSTAINABLE CHEMISTRY AND PHARMACY, 2024, 37
[38]   Optimization of Deep Eutectic-like Solvent-based Ultrasound-assisted Extraction of Polysaccharides from Leonurus Residues [J].
Yuan, Yuan ;
Wei, Liurun ;
Sun, Xiang ;
Sun, Gongbing ;
Ma, Yuzhao ;
Xu, Shengyan ;
He, Jianyu ;
Li, Sidan .
BIORESOURCES, 2024, 19 (02) :2299-2313
[39]   Novel tributyl phosphate-based deep eutectic solvent: Application in microwave assisted extraction of carotenoids [J].
Gorusuk, Emine Munevver ;
Lalikoglu, Melisa ;
Ascl, Yavuz Selim ;
Bener, Mustafa ;
Bekdeser, Burcu ;
Apak, Resat .
FOOD CHEMISTRY, 2024, 459
[40]   Comparison of Conventional Solvent Extraction, Microwave-Assisted Extraction, and Ultrasound-Assisted Extraction Methods for Paclitaxel Recovery from Biomass [J].
Kim, Jin-Hyun .
KOREAN CHEMICAL ENGINEERING RESEARCH, 2020, 58 (02) :273-279
12345