Deep eutectic solvent-based microwave-assisted extraction of genistin, genistein and apigenin from pigeon pea roots

被引：168

作者：

Cui, Qi ^{[1
,2
]}

Peng, Xiao ^{[1
,2
]}

Yao, Xiao-Hui ^{[1
,2
]}

Wei, Zuo-Fu ^{[1
,2
]}

Luo, Meng ^{[1
,2
]}

Wang, Wei ^{[1
,2
]}

Zhao, Chun-Jian ^{[1
,2
]}

Fu, Yu-Jie ^{[1
,2
,3
]}

Zu, Yuan-Gang ^{[1
,2
]}

机构：

[1] Northeast Forestry Univ, Key Lab Forest Plant Ecol, Minist Educ, Harbin 150040, Peoples R China

[2] Northeast Forestry Univ, Engn Res Ctr Forest Biopreparat, Minist Educ, Harbin 150040, Peoples R China

[3] Northeast Forestry Univ, Collaborat Innovat Ctr Dev & Utilizat Forest Reso, Harbin 150040, Peoples R China

来源：

SEPARATION AND PURIFICATION TECHNOLOGY | 2015年 / 150卷

基金：

中国国家自然科学基金;

关键词：

Deep eutectic solvent; Microwave-assisted extraction; Pigeon pea roots; Kinetics; Response surface methodology; PRESSURE CAVITATION EXTRACTION; FLAVONOIDS; OPTIMIZATION; ACID; DRUG;

D O I：

10.1016/j.seppur.2015.06.026

中图分类号：

TQ [化学工业];

学科分类号：

0817 ;

摘要：

The purpose of the study was to develop a new deep eutectic solvent-based microwave-assisted extraction (DES-MAE) method for extracting the three major active compounds genistin, genistein and apigenin from pigeon pea roots. Optimal conditions for DES-MAE, proposed by the single factor and the Box-Behnken design (BBD) tests, were 30% of water in 1,6-hexanediol/ChCl (7:1, mol/mol) as the extraction solvent, microwave power 600W, liquid/solid ratio 14 mL/g, temperature 80 degrees C and time 11 min. The yields of genistin, genistein and apigenin reached 0.449, 0.617 and 0.221 mg/g DW, respectively. The kinetics experiment showed the prominent advantages of DES-MAE such as higher extraction efficiency than other extraction methods. The present results showed that DES could be a kind of green solvent for fast and efficient extraction of the active ingredients from plant materials. (C) 2015 Elsevier B.V. All rights reserved.

引用

页码：63 / 72

页数：10

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