Deep eutectic solvent-based microwave-assisted extraction of genistin, genistein and apigenin from pigeon pea roots

被引：165
作者：
Cui, Qi [1 ,2 ]
Peng, Xiao [1 ,2 ]
Yao, Xiao-Hui [1 ,2 ]
Wei, Zuo-Fu [1 ,2 ]
Luo, Meng [1 ,2 ]
Wang, Wei [1 ,2 ]
Zhao, Chun-Jian [1 ,2 ]
Fu, Yu-Jie [1 ,2 ,3 ]
Zu, Yuan-Gang [1 ,2 ]
机构：
[1] Northeast Forestry Univ, Key Lab Forest Plant Ecol, Minist Educ, Harbin 150040, Peoples R China
[2] Northeast Forestry Univ, Engn Res Ctr Forest Biopreparat, Minist Educ, Harbin 150040, Peoples R China
[3] Northeast Forestry Univ, Collaborat Innovat Ctr Dev & Utilizat Forest Reso, Harbin 150040, Peoples R China
来源：
SEPARATION AND PURIFICATION TECHNOLOGY | 2015年 / 150卷
基金：
中国国家自然科学基金;
关键词：
Deep eutectic solvent; Microwave-assisted extraction; Pigeon pea roots; Kinetics; Response surface methodology; PRESSURE CAVITATION EXTRACTION; FLAVONOIDS; OPTIMIZATION; ACID; DRUG;
D O I：
10.1016/j.seppur.2015.06.026
中图分类号：
TQ [化学工业];
学科分类号：
0817 ;
摘要：
The purpose of the study was to develop a new deep eutectic solvent-based microwave-assisted extraction (DES-MAE) method for extracting the three major active compounds genistin, genistein and apigenin from pigeon pea roots. Optimal conditions for DES-MAE, proposed by the single factor and the Box-Behnken design (BBD) tests, were 30% of water in 1,6-hexanediol/ChCl (7:1, mol/mol) as the extraction solvent, microwave power 600W, liquid/solid ratio 14 mL/g, temperature 80 degrees C and time 11 min. The yields of genistin, genistein and apigenin reached 0.449, 0.617 and 0.221 mg/g DW, respectively. The kinetics experiment showed the prominent advantages of DES-MAE such as higher extraction efficiency than other extraction methods. The present results showed that DES could be a kind of green solvent for fast and efficient extraction of the active ingredients from plant materials. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码：63 / 72
页数：10
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