Pressure-resisting cell for high-pressure, high-resolution nuclear magnetic resonance measurements at very high magnetic fields

被引:57
作者
Yamada, H [1 ]
Nishikawa, K
Honda, M
Shimura, T
Akasaka, K
Tabayashi, K
机构
[1] Kobe Univ, Fac Sci, Dept Chem, Nada Ku, Kobe, Hyogo 6578501, Japan
[2] Kobe Univ, Grad Sch Sci & Technol, Dept Mol Sci, Nada Ku, Kobe, Hyogo 6578501, Japan
关键词
D O I
10.1063/1.1334630
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A pressure-resisting cell system has been developed for high-pressure high-resolution nuclear magnetic resonance (NMR) measurements up to a maximum pressure of 600 MPa. This cell system is capable of performing high-pressure experiments with any standard spectrometer, including modern high field NMR machines. A full description of the high-pressure NMR assembly mounted on a 750 MHz spectrometer is presented along with a detailed explanation of the procedure for preparing the pressure-resisting quartz and glass cells. (C) 2001 American Institute of Physics.
引用
收藏
页码:1463 / 1471
页数:9
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