Crystal structure of bis(N′-((5-(ethoxycarbonyl)-1H-pyrrol-2-yl)methylene)-N-ethylcarbamohydrazonothioato-κ2N,O)nickel(II), C22H30N8O4S2Ni

被引:0
作者
Chen, Kui-Kui [2 ]
Huang, Jing-Tao [1 ]
Lin, Long [1 ]
Wu, Wei-Na [3 ]
机构
[1] Henan Polytech Univ, Sch Mat Sci & Engn, Jiaozuo 454000, Henan, Peoples R China
[2] Shanxi Datong Univ, Coll Min, Datong 037004, Peoples R China
[3] Henan Polytech Univ, Dept Chem & Chem Engn, Jiaozuo 454000, Henan, Peoples R China
来源
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2020年 / 235卷 / 02期
关键词
COMPLEXES;
D O I
10.1515/ncrs-2019-0690
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C22H30N8O4S2Ni, monoclinic, P2(1)/c (no. 14), a = 10.635(2) angstrom, b = 10.308(2) angstrom, c = 12.444(3) angstrom, beta = 101.205(4)degrees, V = 1338.2(5) angstrom(3), Z = 2, R-gt(F) = 0.0417, wR(ref)(F-2) = 0.0937, T = 296(2) K.
引用
收藏
页码:389 / 390
页数:2
相关论文
共 9 条
[1]  
[Anonymous], 2007, SMART SAINT
[2]  
Bermejo E, 2001, Z ANORG ALLG CHEM, V627, P2377, DOI 10.1002/1521-3749(200110)627:10<2377::AID-ZAAC2377>3.0.CO
[3]  
2-O
[4]   Ni(II)/Cu(II) Complexes with Two Pyrrole Thiosemicarbazone Ligands: Crystal Structures and DNA Interaction [J].
Li Xiao-Jing ;
Mao Pan-Dong ;
Wu Wei-Na ;
Kou Kai ;
Liu Shu-Yang ;
Wang Yuan .
CHINESE JOURNAL OF INORGANIC CHEMISTRY, 2017, 33 (07) :1257-1265
[5]   The influence of the substituents at N1 nitrogen on geometry of nickel(II) complexes with heterocyclic thiosemicarbazones [J].
Lobana, Tarlok S. ;
Kumari, Poonam ;
Zeller, Matthias ;
Butcher, Ray J. .
INORGANIC CHEMISTRY COMMUNICATIONS, 2008, 11 (09) :972-974
[6]   Palladium(II) and platinum(II) bis(thiosemicarbazone) complexes of the 2,6-diacetylpyridine series with high cytotoxic activity in cisplatin resistant A2780cisR tumor cells and reduced toxicity [J].
Matesanz, Ana I. ;
Leitao, Ines ;
Souza, Pilar .
JOURNAL OF INORGANIC BIOCHEMISTRY, 2013, 125 :26-31
[7]   In Vitro and in Vivo Anticancer Activity of Copper Bis(thiosemicarbazone) Complexes [J].
Palanimuthu, Duraippandi ;
Shinde, Sridevi Vijay ;
Somasundaram, Kumaravel ;
Samuelson, Ashoka G. .
JOURNAL OF MEDICINAL CHEMISTRY, 2013, 56 (03) :722-734
[8]  
Sheldrick GM, 2015, ACTA CRYSTALLOGR C, V71, P3, DOI [10.1107/S2053273314026370, 10.1107/S2053229614024218, 10.1107/S0108767307043930]
[9]   Design and synthesis of novel N(4)-substituted thiosemicarbazones bearing a pyrrole unit as potential anticancer agents [J].
Zhu, Taofeng ;
Shen, Shanshan ;
Lu, Qin ;
Ye, Xingpei ;
Ding, Weiliang ;
Chen, Ruhua ;
Xie, Jing ;
Zhu, Wenjiao ;
Xu, Jun ;
Jia, Lei ;
Wu, Weina ;
Ma, Tieliang .
ONCOLOGY LETTERS, 2017, 13 (06) :4493-4500