In situ investigation of the fracture of primary carbides and its mechanism in M50 steel

被引:38
作者
Du, Ningyu [1 ,2 ]
Liu, Hanghang [1 ]
Cao, Yanfei [1 ]
Fu, Paixian [1 ]
Sun, Chen [1 ]
Liu, Hongwei [1 ]
Li, Dianzhong [1 ]
机构
[1] Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China
[2] Univ Sci & Technol China, Sch Mat Sci & Engn, Shenyang 110016, Peoples R China
基金
中国国家自然科学基金;
关键词
Bearing steel; Primary carbides; Fracture; X-ray microtomography; MC; FATIGUE-CRACK NUCLEATION; PROPAGATION BEHAVIOR; CLEAVAGE FRACTURE; CYCLE FATIGUE; PARTICLE-SIZE; GRAIN-SIZE; INITIATION; DEFORMATION; SEM;
D O I
10.1016/j.matchar.2022.111822
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The tensile crack initiation and propagation of M50 bearing steel were investigated. It is found that the primary carbides were fractured during the tensile test by in situ SEM, while decohesion of the carbide/matrix interface was hardly observed. In order to capture the initial tensile crack, quasi-in situ X-ray microtomography was performed, indicating that the earliest crack was formed from the broken interior carbides. This indicates that multiple cracks already existed in the matrix when they were observed on the sample surface. Electron backscattered diffraction (EBSD) and the finite element method (FEM) were applied to analyze the fracture behavior of carbide particles. The fracture of carbide particle is produced by the incompatible deformation between the matrix and carbides. The frequency of carbide fracture was found to be related with its fracture strength, size and shape. M2C carbide fracture was more easily broken than the MC carbide during tensile test. In addition, the long axis of most M2C carbides is approximately parallel to its (0001) plane and normal to tensile stress, leading to cracking more easily. Finally, a suggestion of adding pre-deformation is proposed to make M2C carbides broken sufficiently and further refine the primary carbides.
引用
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页数:11
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