Microwave-assisted synthesis of cobalt oxalate nanorods and their thermal conversion to Co3O4 rods

被引：95

作者：

Wang, WW

Zhu, YJ ^{[1
]}

机构：

[1] Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China

[2] Chinese Acad Sci, Grad Sch, Beijing 100864, Peoples R China

来源：

MATERIALS RESEARCH BULLETIN | 2005年 / 40卷 / 11期

基金：

中国国家自然科学基金;

关键词：

nanostructures; oxides; chemical synthesis;

D O I：

10.1016/j.materresbull.2005.06.004

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Cobalt oxalate nanorods have been successfully synthesized by a simple rnicrowave-assisted solution approach using an ionic liquid 1-n-butyl-3-methyl imidazolium tetra flu oroborate. Upon thermal decomposition at 400 degrees C, cobalt oxalate nanorods could be converted to Co3O4 rods consisting of nanoparticles. The products were characterized using X-ray powder diffraction, transmission electron microscopy, thermogravimetric analysis and differential scanning calorimetric analysis. (C) 2005 Elsevier Ltd. All rights reserved.

引用

页码：1929 / 1935

页数：7

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