In situ introduction of dispersed metallic Ag nanoparticles into the channels of mesoporous carbon CMK-3

被引:22
作者
Chen, Ai Bing [1 ]
Zhang, Wei Ping [1 ]
Liu, Yong [1 ]
Han, Xiu Wen [1 ]
Bao, Xin He [1 ]
机构
[1] Chinese Acad Sci, Dalian Inst Chem Phys, State Key Lab Catalysis, Dalian 116023, Peoples R China
基金
中国国家自然科学基金;
关键词
ag nanoparticles; mesoporous carbon; CMK-3; in situ synthesis;
D O I
10.1016/j.cclet.2007.05.038
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
An in situ reduction method has been developed to fabricate metallic Ag nanoparticles inside the channels of mesoporous carbon CMK-3. This approach combines function of the CMK-3 surface by oxidation using HNO3 with the subsequent absorption of Ag+. The resultant nanocomposite materials were characterized by nitrogen adsorption, X-ray diffraction, Auger electron spectroscopy and transmission electron microscopy. Compared with the conventional impregnation method, our approach shows that Ag nanoparticles of 2-4 nm can be uniformly incorporated into CMK-3. (c) 2007 Xin He Bao. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.
引用
收藏
页码:1017 / 1020
页数:4
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