Complete assignments of 1H and 13C NMR spectral data for arylnaphthalene lignana lactones

被引：10
|
作者：
da Silva, Rosangela
Ruas, Marcelo Maia
Donate, Paulo Marcos
机构：
[1] Univ Franca, Nucleo Ciencias Exatas Technol, BR-14404 Fnca, SP, Brazil
[2] Univ Sao Paulo, Fac Filosofia Ciencias & Letras Ribeirao Pret, Dept Quim, BR-14040 Ribeirao Preto, Brazil
来源：
MAGNETIC RESONANCE IN CHEMISTRY | 2007年 / 45卷 / 10期
关键词：
H-1; NMR; C-13; 2D NMR; arylnaphtalene lignan lactone; taiwanin C; 4-methyl dehydroretrodendrin; justicin B;
D O I：
10.1002/mrc.2065
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In this work we describe the complete H-1 and C-13 NMR analyses of three arylnaphtalene lignan lactones (taiwanin C, 4-methyl dehydroretrodendrin and justicidin B) using modern NMR techniques such as gCOSY, nonedited gHSQC, gHMBC and NOE experiments. Complete assignment and homonuclear hydrogen coupling constant measurements were performed. Copyright 2007 John Wiley & Sons, Ltd.
引用
收藏
页码：902 / 904
页数：3
相关论文
共 50 条
  • [41] Complete assignments of the 1H and 13C NMR spectra of six highly functionalized neoclerodane diterpenoids
    Rodríguez, B
    MAGNETIC RESONANCE IN CHEMISTRY, 2001, 39 (03) : 150 - 154
  • [42] Complete assignments of 1H and 13C NMR data of three new dihydrophenanthrofurans from Pleione yunnanensis
    Dong, Hailing
    Wang, Chunlan
    Li, Yan
    Guo, Shunxing
    Yang, Junshan
    MAGNETIC RESONANCE IN CHEMISTRY, 2010, 48 (03) : 256 - 260
  • [43] Spectral assignments and reference data -: 1H, 13C and 15N NMR spectra of ciprofloxacin
    Zieba, A
    Maslankiewicz, A
    Sitkowski, J
    MAGNETIC RESONANCE IN CHEMISTRY, 2004, 42 (10) : 903 - 904
  • [44] Spectral assignments and reference data -: 1H and 13C NMR spectra of N-substituted morpholines
    Katritzky, AR
    Akhmedov, NG
    Yang, HF
    Hall, CD
    MAGNETIC RESONANCE IN CHEMISTRY, 2005, 43 (08) : 673 - 675
  • [45] Complete assignments of 1H and 13C NMR spectroscopic data for three new stigmastane glycosides from Vernonia cumingiana
    Suo, Maorong
    Yang, Junshan
    MAGNETIC RESONANCE IN CHEMISTRY, 2009, 47 (02) : 179 - 183
  • [46] Complete assignments of 1H and 13C NMR spectroscopic data for two new triterpenoid saponins from Ilex pernyi
    Xie, Guang-Bo
    Lei, Lian-Di
    Tu, Peng-Fei
    MAGNETIC RESONANCE IN CHEMISTRY, 2007, 45 (11) : 997 - 1000
  • [47] Complete assignments of 1H and 13C NMR data for two new sesquiterpenes from Cyperus rotundus L.
    Xu, Yan
    Zhang, Hong-Wu
    Wan, Xiao-Chun
    Zou, Zhong-Mei
    MAGNETIC RESONANCE IN CHEMISTRY, 2009, 47 (06) : 527 - 531
  • [48] Complete assignment of 1H and 13C NMR data for nine protopanaxatriol glycosides
    Teng, RW
    Li, HZ
    Chen, JT
    Wang, DZ
    He, YN
    Yang, CR
    MAGNETIC RESONANCE IN CHEMISTRY, 2002, 40 (07) : 483 - 488
  • [49] Conformational evaluation and detailed 1H and 13C NMR assignments of eremophilanolides
    Burgueño-Tapia, E
    Hernández, LR
    Reséndiz-Villalobos, AY
    Joseph-Nathan, P
    MAGNETIC RESONANCE IN CHEMISTRY, 2004, 42 (10) : 887 - 892
  • [50] Separation of floridoside and isofloridosides by HPLC and complete 1H and 13C NMR spectral assignments for D-isofloridoside
    Bondu, Stephanie
    Kervarec, Nelly
    Deslandes, Eric
    Pichon, Roger
    CARBOHYDRATE RESEARCH, 2007, 342 (16) : 2470 - 2473
12345