Solution-combustion: the versatile route to synthesize silver nanoparticles

被引:32
作者
Sharma, Poonam [1 ]
Lotey, Gurmeet Singh [2 ]
Singh, Sukhpreet [3 ]
Verma, N. K. [2 ]
机构
[1] DAV Inst Engn & Technol, Nanotechnol Res Ctr, Jalandhar 144008, India
[2] Thapar Univ, Sch Phys & Mat Sci, Nano Res Lab, Patiala 147004, Punjab, India
[3] Singhania Univ, Dept Chem, Pacheri Bari 333575, Jhunjhunu, India
关键词
Solution-combustion; Silver nanoparticles; Oxidant to fuel ratio; Surface plasmon resonance; NOBLE-METAL NANOPARTICLES; NANOWIRES; CHEMISTRY; PARTICLE; SIZE;
D O I
10.1007/s11051-010-0148-3
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The solution-combustion synthesis (SCS) method was used to prepare silver nanoparticles using glycine and citric acid as fuels. The different combination of fuel to oxidant ratio was used to prepare Ag nanoparticles and its effect on optical spectra, structure and the morphology explored. The purposed method is rapid, effective, cheap and convenient. Silver nanoparticles with different sizes and shapes were synthesized depending upon the different oxidant/fuel ratios. The nanoparticles were characterized using transmission electron microscopy, X-ray diffraction and ultraviolet-visible absorption spectroscopy. Histograms were drawn to compare the mean particle size of synthesized nanoparticles. It was found that citric acid was better fuel as compared to glycine as it results in the more spherical symmetrical nanoparticles, which are supported by various characteristic studies.
引用
收藏
页码:2553 / 2561
页数:9
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