Determination of organic compounds in bottom sediments by gas chromatography/mass spectrometry coupled with static headspace analysis

被引:2
作者
Galaktionova, E. B. [1 ]
Safarova, V. I. [1 ]
Kudasheva, F. Kh. [2 ]
Teplova, G. I. [1 ]
机构
[1] State Analyt Control Bashkortostan Nat Management, Ufa 450104, Bashkortostan, Russia
[2] Bashkyr State Univ, Dept Chem, Ufa 450074, Bashkortostan, Russia
关键词
volatile organic compounds; bottom sediments; gas chromatography/mass spectrometry; headspace analysis;
D O I
10.1134/S1061934812060020
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A procedure is developed for determining volatile organic compounds in bottom sediments by gas chromatography/mass spectrometry coupled to static headspace analysis. The analytical range is 0.004-2.5 mg/kg. The results of analysis of bottom sediments collected from River Belaya in Bashkortostan Republic for volatile organic compounds species are presented. Up to sixteen aromatic and chlorinated aliphatic hydrocarbons were discovered and quantified in the samples collected.
引用
收藏
页码:555 / 559
页数:5
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