Synthesis and electric field-assisted sintering behavior of Al2O3-ZrO2 composite nanopowders by polyacrylamide gel method

被引:3
|
作者
Su, Xinghua [1 ]
Zhou, Jie [1 ]
Wang, Benpan [1 ]
Zhao, Peng [1 ]
机构
[1] Changan Univ, Sch Mat Sci & Engn, Xian 710061, Peoples R China
基金
中国国家自然科学基金; 中国博士后科学基金;
关键词
Al2O3-ZrO2; Nanopowders; Electric field-assisted sintering; Joule heating; CHEMICAL-VAPOR SYNTHESIS; NANOCRYSTALLINE ALPHA-AL2O3; PHASE-TRANSFORMATION; STABILIZED ZIRCONIA; GRAIN-GROWTH; ALUMINA; POWDER; NANOCOMPOSITE; KINETICS; OXIDE;
D O I
10.1007/s10971-016-4085-1
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Al2O3-ZrO2 composite ceramic nanopowders were synthesized using a polyacrylamide gel method. The mean particle size of the Al2O3-ZrO2 nanopowders was found to decrease with increasing mole ratio of monomer to the precursor salt. The Al2O3-ZrO2 nanopowders with mean particle size of 10 nm can be densified in 1 h at 965 A degrees C, by application of a dc electrical field. Under a constant dc electrical field, the current density through the sample of Al2O3-ZrO2 rose rapidly when the temperature increased to a certain value. In the sintering process, the current density was restricted when a sharp increase occurred. It was found that current density had a great effect on the sintering process in electric field-assisted sintering. Joule heating was proposed to be the main mechanism of the electric field-assisted sintering process. The Al2O3-ZrO2 composite ceramic nanopowders were synthesized using a polyacrylamide gel method. The Al2O3-ZrO2 nanopowders can be densified in 1 h at low temperature, by the application of a dc electrical field. Under a constant dc electrical field, the current density through the sample of Al2O3-ZrO2 rose rapidly when the temperature increased to a certain value.
引用
收藏
页码:126 / 132
页数:7
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