Synthesis and characterization of new metal-free and metallophthalocyanines peripherally fused to four 15-membered tetraoxamonoazamacrocycles by microwave irradiation

被引：28

作者：

Kantekin, Halit ^{[1
]}

Biyiklioglu, Zekeriya ^{[1
]}

Celenk, Elif ^{[1
]}

机构：

[1] Karadeniz Tech Univ, Dept Chem, Fac Arts & Sci, TR-61080 Trabzon, Turkey

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2008年 / 11卷 / 06期

关键词：

phthalocyanine; tetraoxamonoazamacrocycle; phthalonitrile; macrocyclization; metallophthalocyanine;

D O I：

10.1016/j.inoche.2008.02.028

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The synthesis and characterization of new metal-free (4) and metallophthalocyanines (5, 6, 7 and 8) substituted four 15-membered tetraoxamonoaza macrocycles from 7-[(4-methylphenyl)sulfonyl]-2,3,6,7,8,9,11,12-octahydro-5H-1,4,10,13,7- benzotetraoxazacyclopen tadecine-15,16-dicarbonitrile (3) is described. The new compounds were characterized by a combination of IR, (1)H NMR, (13)C NMR, UV-vis, elemental analysis and MS spectral data. (C) 2008 Elsevier B.V. All rights reserved.

引用

页码：633 / 635

页数：3

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