N-(2-bromo-1-phenylethyl)-4-methylbenzenesulfonamide

被引:1
作者
Meng, Yue [1 ]
Zhong, Guang-Xiang [1 ]
Hu, Wei-Xiao [1 ]
机构
[1] Zhejiang Univ Technol, Coll Pharmaceut Sci, Hangzhou 310032, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2007年 / 63卷
关键词
D O I
10.1107/S1600536807038445
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C15H16BrNO2S, was obtained unintentionally in our work on the preparation of vicinal haloamine derivatives. The molecule lies across a crystallographic mirror plane with the NH group disordered across this mirror plane. The dihedral angle between the benzene and phenyl rings is 25.10 (17)degrees. In the crystal structure, intermolecular N-H center dot center dot center dot O hydrogen bonds link the molecules into chains running along the b axis. In addition, C-H center dot center dot center dot Br hydrogen bonds are observed.
引用
收藏
页码:O3744 / U2437
页数:9
相关论文
共 6 条
  • [1] COMPLETION AND REFINEMENT OF CRYSTAL-STRUCTURES WITH SIR92
    ALTOMARE, A
    CASCARANO, G
    GIACOVAZZO, C
    GUAGLIARDI, A
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1993, 26 (pt 3) : 343 - 350
  • [2] BRUKER, 2005, SAINT SHELXTL
  • [3] Bruker, 2005, APEX2
  • [4] Sheldrick G. M., 1996, SADABS PROGRAM EXPIR
  • [5] Sheldrick GM, 2015, ACTA CRYSTALLOGR C, V71, P3, DOI [10.1107/S2053229614024218, 10.1107/S0108767307043930]
  • [6] Transition metal-catalyzed regio- and stereoselective aminobromination of olefins with TsNH2 and NBS as nitrogen and bromine sources
    Thakur, VV
    Talluri, SK
    Sudalai, A
    [J]. ORGANIC LETTERS, 2003, 5 (06) : 861 - 864