Large-pore mesoporous nanocrystalline titania thin films synthesized through evaporation-induced self-assembly

被引:48
|
作者
Liu, KS
Zhang, ML
Shi, KY
Fu, HG [1 ]
机构
[1] Heilongjiang Univ, Sch Chem & Mat Sci, Phys Chem Lab, Harbin 150080, Peoples R China
[2] Harbin Engn Univ, Sch Chem Engn, Harbin 150001, Peoples R China
基金
美国国家科学基金会; 中国国家自然科学基金;
关键词
mesoporous titania; thin film; anatase; evaporation induced self-assembly (EISA);
D O I
10.1016/j.matlet.2005.05.062
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Mesoporous nanocrystalline TiO2 thin films with a large-pore diameter (up to 14 nm), narrow pore-size distribution have been synthesized by using tetrabutyl titanate as the inorganic precursor and triblock copolymer (Pluronic P123) as the structure-directing agent under acidic conditions. The synthetic method is based on the well-documented evaporation-induced self-assembly (EISA). The mesopore size of obtained samples can be adjusting by altering the inorganic source/surfactant mass ratio. The resulting materials were characterized by XRD, AFM, and nitrogen adsorption-desorption. (C) 2005 Elsevier B.V. All rights reserved.
引用
收藏
页码:3308 / 3310
页数:3
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