Large-pore mesoporous nanocrystalline titania thin films synthesized through evaporation-induced self-assembly

被引:48
|
作者
Liu, KS
Zhang, ML
Shi, KY
Fu, HG [1 ]
机构
[1] Heilongjiang Univ, Sch Chem & Mat Sci, Phys Chem Lab, Harbin 150080, Peoples R China
[2] Harbin Engn Univ, Sch Chem Engn, Harbin 150001, Peoples R China
基金
美国国家科学基金会; 中国国家自然科学基金;
关键词
mesoporous titania; thin film; anatase; evaporation induced self-assembly (EISA);
D O I
10.1016/j.matlet.2005.05.062
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Mesoporous nanocrystalline TiO2 thin films with a large-pore diameter (up to 14 nm), narrow pore-size distribution have been synthesized by using tetrabutyl titanate as the inorganic precursor and triblock copolymer (Pluronic P123) as the structure-directing agent under acidic conditions. The synthetic method is based on the well-documented evaporation-induced self-assembly (EISA). The mesopore size of obtained samples can be adjusting by altering the inorganic source/surfactant mass ratio. The resulting materials were characterized by XRD, AFM, and nitrogen adsorption-desorption. (C) 2005 Elsevier B.V. All rights reserved.
引用
收藏
页码:3308 / 3310
页数:3
相关论文
共 50 条
  • [1] Tuning the pore size and structure of mesoporous carbons synthesized using an evaporation-induced self-assembly method
    Li, Peng
    Song, Yan
    Guo, Quangui
    Shi, Jingli
    Liu, Lang
    MATERIALS LETTERS, 2011, 65 (14) : 2130 - 2132
  • [2] Preparation of ordered multilayer titania/polymer nanocomposite thin films by evaporation-induced self-assembly
    Zhang, SM
    He, BF
    Zhang, ZJ
    Dang, HX
    Liu, WM
    Xue, QJ
    CHEMISTRY LETTERS, 2004, 33 (11) : 1498 - 1499
  • [3] Synthesis of large-pore phenyl-bridged mesoporous organosilica with thick walls by evaporation-induced self-assembly for efficient benzene adsorption
    Hao, Na
    Yang, Yunxia
    Wang, Huanting
    Webley, Paul A.
    Zhao, Dongyuan
    JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2010, 346 (02) : 429 - 435
  • [4] Highly-ordered mesoporous nanocrystalline yttria-stabilized zirconia synthesized through evaporation-induced self-assembly method
    Hung, I-Ming
    Hung, De-Tsai
    Fung, Kuan-Zong
    Hon, Min-Hsiung
    MATERIALS LETTERS, 2008, 62 (6-7) : 1147 - 1150
  • [5] Formation Mechanism of Cubic Mesoporous Carbon Monolith Synthesized by Evaporation-Induced Self-assembly
    Florent, Marc
    Xue, Chunfeng
    Zhao, Dongyuan
    Goldfarb, Daniella
    CHEMISTRY OF MATERIALS, 2012, 24 (02) : 383 - 392
  • [6] Preparation, characterization, and photo-induced hydrophilicity of nanocrystalline anatase thin films synthesized through evaporation-induced assembly
    Liu, KS
    Zhang, ML
    Zhou, W
    Li, L
    Wang, J
    Fu, HG
    NANOTECHNOLOGY, 2005, 16 (12) : 3006 - 3011
  • [7] Evaporation-induced self-assembly of periodic mesoporous organosilica thin films by sol-gel process
    Wang Jianfang
    Zhang Xueao
    Tian Tian
    Wu Wenjian
    RARE METAL MATERIALS AND ENGINEERING, 2008, 37 : 209 - 212
  • [8] Facile synthesis of mesoporous ZnAl2O4 thin films through the evaporation-induced self-assembly method
    Tian, Xiqiang
    Wan, Lijuan
    Pan, Kai
    Tian, Chungui
    Fu, Honggang
    Shi, Keying
    Journal of Alloys and Compounds, 2009, 488 (01): : 320 - 324
  • [9] Facile synthesis of mesoporous ZnAl2O4 thin films through the evaporation-induced self-assembly method
    Tian, Xiqiang
    Wan, Lijuan
    Pan, Kai
    Tian, Chungui
    Fu, Honggang
    Shi, Keying
    JOURNAL OF ALLOYS AND COMPOUNDS, 2009, 488 (01) : 320 - 324
  • [10] Fundamentals of mesostructuring through evaporation-induced self-assembly
    Grosso, D
    Cagnol, F
    Soler-Illia, GJDA
    Crepaldi, EL
    Amenitsch, H
    Brunet-Bruneau, A
    Bourgeois, A
    Sanchez, C
    ADVANCED FUNCTIONAL MATERIALS, 2004, 14 (04) : 309 - 322