A fast-cooling sample-positioning probe for low-temperature neutron scattering experiments

被引:2
作者
Manning, Andrew [1 ]
Avdeev, Maxim [1 ]
Imperia, Paolo [1 ]
机构
[1] Australian Nucl Sci & Technol Org, Australian Ctr Neutron Scattering, Sydney, NSW, Australia
关键词
cryostats; cryogenics; neutron scattering; sample environment; CRYOSTAT; SYSTEM;
D O I
10.1107/S1600576719016704
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Top-loading exchange gas cryostats have for a long time been a widely used sample environment device for a variety of neutron scattering experiments. In particular, they allow for simpler and faster changes of samples mounted on sample-positioning probes than is possible with bottom-loading cryostats under vacuum. Here, a new design for sample probes using composite materials is investigated, which significantly decreases the time required to cool a newly installed sample in two different types of closed-cycle exchange gas cryostat.
引用
收藏
页码:297 / 301
页数:5
相关论文
共 6 条
[1]   ECHIDNA: a decade of high-resolution neutron powder diffraction at OPAL [J].
Avdeev, Maxim ;
Hester, James R. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2018, 51 :1597-1604
[2]  
Brochier D., 1977, 7774 ILL
[3]   Cryogen-free cryostat for neutron scattering sample environment [J].
Chapman, C. R. ;
Evans, B. E. ;
Dudman, M. P. ;
Keeping, J. ;
Down, R. B. E. ;
Kirichek, O. ;
Bowden, Z. A. .
CRYOGENICS, 2011, 51 (03) :146-149
[4]  
Ekin JackW., 2011, Experimental Techniques for low temperature measurements: Cryostat Design, Material Properties, and Superconductor Critical-Current Testing p41
[5]   Powder sample-positioning system for neutron scattering allowing gas delivery in top-loading cryofurnaces [J].
Lee, Stanley ;
Chevreau, Hubert ;
Booth, Norman ;
Duyker, Samuel G. ;
Ogilvie, Stephen H. ;
Imperia, Paolo ;
Peterson, Vanessa K. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2016, 49 :705-711
[6]   Safety interlock and vent system to alleviate potentially dangerous ice blockage of top-loading cryostat sample sticks [J].
Pangelis, S. ;
Olsen, S. R. ;
Scherschligt, J. ;
Leao, J. B. ;
Pullen, S. A. ;
Dender, D. ;
Hester, J. R. ;
Imperia, P. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2013, 46 :1236-1239