Synthesis of SnO2 micro-spheres, nano-rods and nano-flowers via simple hydrothermal route

被引:31
作者
Dang Duc Vuong [1 ]
Vu Xuan Hien [1 ]
Khuc Quang Trung [1 ,2 ]
Nguyen Duc Chien [1 ]
机构
[1] Hanoi Univ Sci & Technol, Inst Engn Phys, Hanoi, Vietnam
[2] Univ Fire Fighting & Protect, Hanoi, Vietnam
关键词
GAS-SENSING PROPERTIES; LARGE-SCALE; THIN-FILMS; TIN OXIDE; GROWTH; ZNO; ARRAYS; TEMPERATURE; PROPERTY; SIZE;
D O I
10.1016/j.physe.2011.06.022
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
SnO2 micro-spheres (0.5 - 2 mu m diameter), nano-flowers (petal size: 100-250 nm diameter; 500 nm 2 mu m length) and nano-rods (3-6 nm diameter; 10-30 nm length) were synthesized by hydrothermal route. The samples were characterized by field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and X-ray diffraction (XRD). The influence of precursor, hydrothermal temperature and treatment time on the formation of SnO2 multi-morphology was also investigated. Moreover, a possible formation mechanism and relationships among morphologies were discussed. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码:345 / 349
页数:5
相关论文
共 35 条
[21]   Controlled c-oriented ZnO nanorod arrays and m-plane ZnO thin film growth on Si substrate by a hydrothermal method [J].
Shi, Yuanyuan ;
Yang, Zhan ;
Cao, Hongtao ;
Liu, Zhimin .
JOURNAL OF CRYSTAL GROWTH, 2010, 312 (04) :568-572
[22]   Modulated TiO2 nanotube stacks and their use in interference sensors [J].
Song, Yan-Yan ;
Schmuki, Patrik .
ELECTROCHEMISTRY COMMUNICATIONS, 2010, 12 (04) :579-582
[23]   On the correlation between morphology and gas sensing properties of RGTO SnO2 thin films [J].
Szuber, J ;
Uljanow, J ;
Karczewska-Buczek, T ;
Jakubik, W ;
Waczynski, K ;
Kwoka, M ;
Konczak, S .
THIN SOLID FILMS, 2005, 490 (01) :54-58
[24]   The effect of seed layer on morphology of ZnO nanorod arrays grown by hydrothermal method [J].
Tao, Yinglei ;
Fu, Ming ;
Zhao, Ailun ;
He, Dawei ;
Wang, Yongsheng .
JOURNAL OF ALLOYS AND COMPOUNDS, 2010, 489 (01) :99-102
[25]   Hydrogen sulfide gas sensing properties of thin films derived from SnO2 sols different in grain size [J].
Vuong, DD ;
Sakai, G ;
Shimanoe, K ;
Yamazoe, N .
SENSORS AND ACTUATORS B-CHEMICAL, 2005, 105 (02) :437-442
[26]   Synthesis and gas sensitivities of SnO2 nanorods and hollow microspheres [J].
Wang, Hazhen ;
Liang, Jianbo ;
Fan, Hai ;
Xi, Baojuan ;
Zhang, Maofeng ;
Xiong, Shenglin ;
Zhu, Yongchun ;
Qian, Yitai .
JOURNAL OF SOLID STATE CHEMISTRY, 2008, 181 (01) :122-129
[27]   SnO2 nanorods and hollow spheres: Controlled synthesis and gas sensing properties [J].
Xu Jiaqiang ;
Wang Ding ;
Qin Lipeng ;
Yu Weijun ;
Pan Qingyi .
SENSORS AND ACTUATORS B-CHEMICAL, 2009, 137 (02) :490-495
[28]   SnO2 quantum dots and quantum wires:: Controllable synthesis, self-assembled 2D architectures, and gas-sensing properties [J].
Xu, Xiangxing ;
Zhuang, Jing ;
Wang, Xun .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2008, 130 (37) :12527-12535
[29]   Growth of ZnO nanorod forests and characterization of ZnO-coated nylon fibers [J].
Xue, Chao-Hua ;
Wang, Rui-Li ;
Zhang, Jing ;
Jia, Shun-Tian ;
Tian, Li-Qiang .
MATERIALS LETTERS, 2010, 64 (03) :327-330
[30]   Diameter-controlled growth of TiO2 nanotube arrays by anodization and its photoelectric property [J].
Yang, Han ;
Pan, Chunxu .
JOURNAL OF ALLOYS AND COMPOUNDS, 2010, 492 (1-2) :L33-L35