Synthesis of SnO2 micro-spheres, nano-rods and nano-flowers via simple hydrothermal route

被引:31
作者
Dang Duc Vuong [1 ]
Vu Xuan Hien [1 ]
Khuc Quang Trung [1 ,2 ]
Nguyen Duc Chien [1 ]
机构
[1] Hanoi Univ Sci & Technol, Inst Engn Phys, Hanoi, Vietnam
[2] Univ Fire Fighting & Protect, Hanoi, Vietnam
关键词
GAS-SENSING PROPERTIES; LARGE-SCALE; THIN-FILMS; TIN OXIDE; GROWTH; ZNO; ARRAYS; TEMPERATURE; PROPERTY; SIZE;
D O I
10.1016/j.physe.2011.06.022
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
SnO2 micro-spheres (0.5 - 2 mu m diameter), nano-flowers (petal size: 100-250 nm diameter; 500 nm 2 mu m length) and nano-rods (3-6 nm diameter; 10-30 nm length) were synthesized by hydrothermal route. The samples were characterized by field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and X-ray diffraction (XRD). The influence of precursor, hydrothermal temperature and treatment time on the formation of SnO2 multi-morphology was also investigated. Moreover, a possible formation mechanism and relationships among morphologies were discussed. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码:345 / 349
页数:5
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