Naturally Derived Allylated Gallic Acid for Interfacially Polymerized Membranes

被引:5
作者
Alhazmi, Banan [1 ,2 ]
Alduraiei, Fadhilah [1 ,2 ]
Manchanda, Priyanka [1 ,2 ]
Chisca, Stefan [1 ,2 ]
Szekely, Gyorgy [2 ,3 ]
Nunes, Suzana P. [1 ,2 ]
机构
[1] King Abdullah Univ Sci & Technol KAUST, Environm Sci & Technol Biol & Environm Sci & Engn, Thuwal 239556900, Saudi Arabia
[2] King Abdullah Univ Sci & Technol KAUST, Adv Membrane & Porous Mat Ctr, Thuwal 239556900, Saudi Arabia
[3] King Abdullah Univ Sci & Technol KAUST, Chem Sci Phys Sci & Engn Div, Thuwal 239556900, Saudi Arabia
关键词
green chemistry; natural precursor; interfacial polymerization; nanofiltration; thin film; NANOFILTRATION MEMBRANES; PHYSIOCHEMICAL PROPERTIES; PERFORMANCE; CHEMISTRY; POLYAMIDE; FTIR; XPS;
D O I
10.1021/acssuschemeng.2c02637
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A naturally derived monomer, allylated gallic acid (AG), was herein proposed as a monomer for interfacially polymerized thin-film composite nanofiltration membranes. We investigated the synthesis of the thin-film composite polyester membranes by varying the concentration of the AG monomer and the reaction time with trimesoyl chloride. In addition, we demonstrated the synthesis of a polyesteramide film using a mixture of AG and m-phenylene diamine, although there are a few orders of magnitude differences in their reactivity. While membranes prepared using the classical polyamide process had a water permeance of 0.54 L m(-2) h(-1). bar(-1) , the prepared polyesteramide and polyester films had water permeances of 12.3 and 47.6 L m(-2) bar(-1) , respectively The rejection of dyes was larger than 700 g mor(-1) and could be tuned to 327 g mol(-1) by changing the chemical composition and reaction time. The retention of inorganic salts followed the order Na2SO4 > MgSO4 approximate to NaCl. Therefore, the membrane performance demonstrates the potential of the phenolic monomer to be integrated into the synthesis of thin-film composite membranes. Besides, the availability of the free allyl group holds potential for further modification and covalent binding onto the surface.
引用
收藏
页码:13585 / 13594
页数:10
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