Sequential Thermal Dissolution of Huolinguole Lignite in Methanol and Ethanol

被引：146

作者：

Lu, Hai-Yun ^{[1
]}

Wei, Xian-Yong ^{[1
]}

Yu, Rui ^{[1
]}

Peng, Yao-Li ^{[1
]}

Qi, Xing-Zhen ^{[1
]}

Qie, Li-Man ^{[1
]}

Wei, Qing ^{[1
]}

Lv, Jie ^{[1
]}

Zong, Zhi-Min ^{[1
]}

Zhao, Wei ^{[1
]}

Zhao, Yun-Peng ^{[1
]}

Ni, Zhong-Hai ^{[1
]}

Wu, Lin ^{[2
]}

机构：

[1] China Univ Min & Technol, Minist Educ, Key Lab Coal Proc & Efficient Utilizat, Xuzhou 221008, Jiangsu, Peoples R China

[2] Wuhan Univ Sci & Technol, Hubei Coal Convers & New Carbon Mat Key Lab, Wuhan 430081, Hubei, Peoples R China

来源：

ENERGY & FUELS | 2011年 / 25卷 / 06期

基金：

中国国家自然科学基金;

关键词：

PROMOTED H-DONATION; EXTRACTION YIELD; SOLVENT-EXTRACTION; FUNCTIONAL-GROUPS; COAL CONVERSION; ASHLESS COAL; DONOR MEDIA; HYPERCOAL; TEMPERATURE; ALCOHOLS;

D O I：

10.1021/ef101734f

中图分类号：

TE [石油、天然气工业]; TK [能源与动力工程];

学科分类号：

0807 ; 0820 ;

摘要：

The sequential thermal dissolution of huolinguole lignite in methanol and ethanol was reported. HL was pulverized to pass through a 200-mesh sieve followed by drying in a vacuum at 80°C for 48 h. The 4 g of HL and 30 mL of methanol or ethanol were put into a 100 mL stainless-steel, magnetically stirred autoclave and after drawing most of the air out from the autoclave with a vacuum pump at room temperature, the autoclave was heated to 200° C and maintained at that temperature for 2 h. The autoclave was cooled to room temperature in a water bath, and the reaction mixture (RM1) was taken out from the autoclave and filtrated to separate RM1 into filtrate (F1) and filter cake (FC1). The significant increases in total yields (TY) of methanol-extractable fraction (MEF) and ethanol-extractable fraction (EEF) were initiated from 270 and 240° C and reached 23.0 and 55.3% at 330° C, respectively.

引用

页码：2741 / 2745

页数：5

共 39 条

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