Synthesis and characterization of silicon-containing poly(amide-amide)s

被引：0

作者：

Joshi, MD ^{[1
]}

Lonikar, SV ^{[1
]}

Maldar, NN ^{[1
]}

机构：

[1] Shivaji Univ, Ctr Postgrad Studies, Dept Chem, Solapur 413003, India

来源：

JOURNAL OF APPLIED POLYMER SCIENCE | 2001年 / 79卷 / 09期

关键词：

bis[(4-carboxyphenyl) 4-benzamide] dimethylsilane; aromatic diamines; silicon-containing poly(amide-amide)s; solubility and thermal properties;

D O I：

10.1002/1097-4628(20010228)79:9<1610::AID-APP100>3.0.CO;2-E

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

A modified new aromatic diacid, bis[(4-carboxyphenyl) 4-benzamide] dimethylsilane (TV) with preformed amide linkages and a silicon moiety was synthesized and characterized by IR, NMR, mass spectroscopy, and a physical constant. Novel poly(amide-amide)s were synthesized from IV and aromatic diamines by Yamazaki's direct polyamidation method in N-methyl pyrrolidinone. The polymers were obtained in excellent yields and showed reduced viscosities in the range of 0.42-6.15 dL/g. They were readily soluble in aprotic polar solvents. These poly(amide-amide)s showed glass-transition temperatures of 303-378 degreesC as measured by DSC and showed no weight loss below 377 degreesC in a nitrogen atmosphere. (C) 2000 John Wiley & Sons, Inc.

引用

页码：1610 / 1617

页数：8

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