Green synthesis, morphological and optical studies of CuO nanoparticles

被引:183
作者
Reddy, K. Rayapa [1 ]
机构
[1] Andhra Loyola Coll, Dept Chem, Vijayawada, Andhra Pradesh, India
关键词
Green method; Nanoparticle; Optical properties; EDX; Band gap energy; COPPER NANOPARTICLES; OXIDE NANOPARTICLES; THERMAL-DECOMPOSITION; POLYMER COMPOSITES; SILVER; GOLD;
D O I
10.1016/j.molstruc.2017.09.005
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
CuO nanoparticles were synthesized by environmentally benign green route with copper acetate precursor using Caloropis procera leaf extract. The CuO nanoparticles produced by the process after calcination at 700 degrees C were characterized by X-ray diffraction (XRD) and the pattern reveals monoclinic structure. The cylindrical shape of CuO nanoparticles were observed by scanning electron microscopy. FT-IR spectra confirmed the adsorption of surfactant molecules at the surface of CuO nanoparticles and presence of Cu-O bonding. Thermal studies were carried out by thermogravimetric and deferential thermal analysis techniques. Raman spectra, is used to explore the local atomic arrangements and vibrations of CuO nanoparticles. In addition, UV-Visible spectra were used to estimate the band gap energy of CuO nanoparticles. (C) 2017 Elsevier B.V. All rights reserved.
引用
收藏
页码:553 / 557
页数:5
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