System development, formability quality and microstructure evolution of selective laser-melted magnesium

被引:86
作者
Yang, Youwen [1 ]
Wu, Ping [2 ]
Lin, Xin [3 ]
Liu, Yong [4 ]
Bian, Hong [5 ]
Zhou, Yuanzhuo [1 ]
Gao, Chengde [1 ]
Shuai, Cijun [1 ]
机构
[1] Cent S Univ, State Key Lab High Performance Complex Mfg, Changsha, Hunan, Peoples R China
[2] Xiangtan Univ, Coll Chem, Xiangtan, Peoples R China
[3] Northwestern Polytech Univ, State Key Lab Solidificat Proc, Xian, Peoples R China
[4] Cent S Univ, State Key Lab Powder Met, Changsha, Hunan, Peoples R China
[5] Hunan Farsoon High Technol Co Ltd, Changsha, Hunan, Peoples R China
基金
中国国家自然科学基金;
关键词
Selective laser melting; system development; microstructure; magnesium; degradation; ZN-ZR ALLOY; BONE; BIOMATERIALS; BEHAVIOR; APATITE; POWDER; CA;
D O I
10.1080/17452759.2016.1210522
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A selective laser melting (SLM) system, which consisted of a fibre laser, a three-dimensional motion platform and a motion control system, was developed in this study. The effect of process parameters on the microstructure evolution of SLMed magnesium parts was investigated. The results revealed that under an irradiation of laser energy density <3.0 J/mm, the powder remained in the discrete state. At a laser energy density 3.0-6.0 J/mm, the powder partially melted and sintered together, yielding incompact tracks. As the energy density increased to 6.0-12.0 J/mm, the powder fully melted forming continuous and smooth tracks. With a further increase in the laser energy density evaporation of the powder occurred. Dense magnesium parts free of pores and cracks were successfully fabricated with the optimal energy density of 10.0 J/mm. The immersion experiment revealed that the degradation product was mainly consisted of Mg(OH)(2), which slowed down the degradation rate acting as a protective layer.
引用
收藏
页码:173 / 181
页数:9
相关论文
共 24 条
[1]   Magnesium alloys development towards the 21st century [J].
Aghion, E ;
Bronfin, B .
MAGNESIUM ALLOYS 2000, 2000, 350-3 :19-28
[2]  
[Anonymous], 2004, E804 ASTM
[3]   Corrosion mechanism applicable to biodegradable magnesium implants [J].
Atrens, Andrej ;
Liu, Ming ;
Abidin, Nor Ishida Zainal .
MATERIALS SCIENCE AND ENGINEERING B-ADVANCED FUNCTIONAL SOLID-STATE MATERIALS, 2011, 176 (20) :1609-1636
[4]   In vivo study of magnesium plate and screw degradation and bone fracture healing [J].
Chaya, Amy ;
Yoshizawa, Sayuri ;
Verdelis, Kostas ;
Myers, Nicole ;
Costello, Bernard J. ;
Chou, Da-Tren ;
Pal, Siladitya ;
Maiti, Spandan ;
Kumta, Prashant N. ;
Sfeir, Charles .
ACTA BIOMATERIALIA, 2015, 18 :262-269
[5]   Optimization of annealing treatment parameters in a twin roll cast and warm rolled ZK60 alloy sheet [J].
Chen, Hongmei ;
Yu, Huashun ;
Kang, Suk Bong ;
Cho, Jae Hyoung ;
Min, Guanghui .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2010, 527 (4-5) :1236-1242
[6]   Laser additive manufacturing of metallic components: materials, processes and mechanisms [J].
Gu, D. D. ;
Meiners, W. ;
Wissenbach, K. ;
Poprawe, R. .
INTERNATIONAL MATERIALS REVIEWS, 2012, 57 (03) :133-164
[7]   Selective laser melting additive manufacturing of Inconel 718 superalloy parts: Densification, microstructure and properties [J].
Jia, Qingbo ;
Gu, Dongdong .
JOURNAL OF ALLOYS AND COMPOUNDS, 2014, 585 :713-721
[8]   Biomimetic apatite formation on chemically treated titanium [J].
Jonásová, L ;
Müller, FA ;
Helebrant, A ;
Strnad, J ;
Greil, P .
BIOMATERIALS, 2004, 25 (7-8) :1187-1194
[9]   Influence of Ca on the corrosion properties of magnesium for biomaterials [J].
Kim, Woo-Cheol ;
Kim, Jung-Gu ;
Lee, Ji-Young ;
Seok, Hyun-Kwang .
MATERIALS LETTERS, 2008, 62 (25) :4146-4148
[10]   Formation of biologically active bone-like apatite on metals and polymers by a biomimetic process [J].
Kokubo, T .
THERMOCHIMICA ACTA, 1996, 280 :479-490