Determination of volatile compounds in whiting (Merlangius merlangus) using headspace-solid-phase microextraction-gas chromatography-mass spectrometry

被引：17
|
作者：
Duflos, G [1 ]
Moine, F [1 ]
Coin, VM [1 ]
Malle, P [1 ]
机构：
[1] Agence Francaise Secur Sanitaire Aliments, Lab Etude & Rech Produits Peche, F-62200 Boulogne, France
来源：
JOURNAL OF CHROMATOGRAPHIC SCIENCE | 2005年 / 43卷 / 06期
关键词：
D O I：
10.1093/chromsci/43.6.304
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A method using headspace-solid-phase microextraction-gas chromatography-mass spectrometry to extract volatile compounds from whiting is developed. Several parameters such as sorption time, desorption time, fiber type, and matrix form are optimized to achieve better sensitivity in minimal analysis time. The efficiency of the method is determined by the linear range and repeatability; a mean relative standard deviation of approximately 7% is measured. It was possible to identify and quantitate 30 volatile compounds of interest present in spoiled whiting.
引用
收藏
页码：304 / 312
页数：9
相关论文
共 50 条
  • [31] Determination of terpenes in tequila by solid phase microextraction-gas chromatography-mass spectrometry
    Pena-Alvarez, Araceli
    Capella, Santiago
    Juarez, Rocio
    Labastida, Carmen
    JOURNAL OF CHROMATOGRAPHY A, 2006, 1134 (1-2) : 291 - 297
  • [32] Headspace solid-phase microextraction-gas chromatography-mass spectrometry for profiling free volatile compounds in Cabernet Sauvignon grapes and wines
    Canuti, Valentina
    Conversano, Michael
    Calzi, Marco Li
    Heymann, Hildegarde
    Matthews, Mark A.
    Ebeler, Susan E.
    JOURNAL OF CHROMATOGRAPHY A, 2009, 1216 (15) : 3012 - 3022
  • [33] Determination of 2-Methylisoborneol and Geosmin in Water by Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry
    Kou Li-Juan
    Liang Chun-Shi
    Wei Shu-Long
    Zang Jin-Hai
    Cai Liu-Yan
    CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2011, 39 (12) : 1932 - 1933
  • [34] Determination of ethylphenols in wine by in situ derivatisation and headspace solid-phase microextraction-gas chromatography-mass spectrometry
    Carrillo, Jose David
    Tena, Maria Teresa
    ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2007, 387 (07) : 2547 - 2558
  • [35] Determination of off-flavour compounds in apple juice caused by microorganisms using headspace solid phase microextraction-gas chromatography-mass spectrometry
    Zierler, B
    Siegmund, B
    Pfannhauser, W
    ANALYTICA CHIMICA ACTA, 2004, 520 (1-2) : 3 - 11
  • [36] Improvement of a headspace solid phase microextraction-gas chromatography/mass spectrometry method for the analysis of wheat bread volatile compounds
    Raffo, Antonio
    Carcea, Marina
    Castagna, Claudia
    Magri, Andrea
    JOURNAL OF CHROMATOGRAPHY A, 2015, 1406 : 266 - 278
  • [37] Determination of homocysteine and its related compounds by solid-phase microextraction-gas chromatography-mass spectrometry
    Myung, SW
    Kim, M
    Min, HK
    Yoo, FA
    Kim, KR
    JOURNAL OF CHROMATOGRAPHY B, 1999, 727 (1-2): : 1 - 8
  • [38] Analysis of Volatile Compounds in Different Varieties of Plum Fruits Based on Headspace Solid-Phase Microextraction-Gas Chromatography-Mass Spectrometry Technique
    Zhang, Qin
    Zhu, Shouliang
    Lin, Xin
    Peng, Junsen
    Luo, Dengcan
    Wan, Xuan
    Zhang, Yun
    Dong, Xiaoqing
    Ma, Yuhua
    HORTICULTURAE, 2023, 9 (10)
  • [39] Analysis of Volatile Organic Compounds in Black Jujube by Heaspace-Gas Chromatography-Ion Mobility Spectrometry and Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry
    Wang Y.
    Wang L.
    Wang Y.
    Shipin Kexue/Food Science, 2022, 43 (08): : 247 - 254
  • [40] Headspace solid-phase microextraction and gas chromatography-mass spectrometry analysis of free volatile compounds inMango
    Chunqing Shang
    Chunhui Deng
    Xiaoyue Zhang
    Zhengfu Chen
    Yaoming Hu
    Chromatographia, 2002, 55 : 737 - 741
12345