Electrodeposition and characterization of PbSe films on indium tin oxide glass substrates

被引:33
作者
Li, KW [1 ]
Meng, XT [1 ]
Liang, X [1 ]
Wang, H [1 ]
Yan, H [1 ]
机构
[1] Beijing Univ Technol, Coll Mat Sci & Engn, Beijing 100022, Peoples R China
关键词
PbSe; electrodeposition; Raman scattering;
D O I
10.1007/s10008-005-0660-z
中图分类号
O646 [电化学、电解、磁化学];
学科分类号
081704 ;
摘要
Electrodeposition of lead selenide (PbSe) thin films on indium tin oxide (ITO) covered glass is described. While disodium salt of ethylenediaminetetraaceticacid was used to complex the lead ions, well crystallized, nearly stoichiometric and mirror-like PbSe films were deposited on ITO glass in potentiostatic mode using aqueous acidic electrolyte containing Pb and Se precursors at different bath temperature. The improvement of crystallinity of the PbSe films deposited at different temperature was studied using X-ray diffraction and Raman scattering. The morphology and composition of the films were characterized by scanning electron microscopy and energy disperse analysis by X-ray, respectively. The optical property of the film was studied by optical measurement techniques.
引用
收藏
页码:48 / 53
页数:6
相关论文
共 18 条
[1]  
DAS VD, 1990, J MATER SCI-MATER EL, V1, P169, DOI 10.1007/BF00696071
[2]   Electrodeposition of EuSe thin films onto different substrates [J].
Gaikwad, NS ;
Bhosale, CH .
MATERIALS CHEMISTRY AND PHYSICS, 2002, 76 (02) :198-203
[3]   A simple solution growth technique for PbSe thin films [J].
Grozdanov, I ;
Najdoski, M ;
Dey, SK .
MATERIALS LETTERS, 1999, 38 (01) :28-32
[4]   BAND STRUCTURE PARAMETERS DEDUCED FROM TUNNELING EXPERIMENTS [J].
HALL, RN ;
RACETTE, JH .
JOURNAL OF APPLIED PHYSICS, 1961, 32 :2078-&
[6]   Raman scattering investigation on the phase evolution of ferroelectric lead barium niobate [J].
Lanciotti, F ;
Pizani, PS ;
Santos, IA ;
do Carmo, CV ;
Garcia, D ;
Eiras, JA .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 2001, 62 (07) :1247-1250
[7]   Sonochemical synthesis of silver, copper and lead selenides [J].
Li, B ;
Xie, Y ;
Huang, J ;
Qian, Y .
ULTRASONICS SONOCHEMISTRY, 1999, 6 (04) :217-220
[8]   RAMAN EFFECT IN CRYSTALS [J].
LOUDON, R .
ADVANCES IN PHYSICS, 1964, 13 (52) :423-&
[9]   ELECTROCHEMICAL DEPOSITION OF PBSE THIN-FILMS FROM AQUEOUS-SOLUTIONS [J].
MOLIN, AN ;
DIKUSAR, AI .
THIN SOLID FILMS, 1995, 265 (1-2) :3-9
[10]   ELECTRODEPOSITION OF ZINC SELENIDE [J].
NATARAJAN, C ;
SHARON, M ;
LEVYCLEMENT, C ;
NEUMANNSPALLART, M .
THIN SOLID FILMS, 1994, 237 (1-2) :118-123