GREEN SYNTHESIS OF COPPER NANOPARTICLES FROM MYRTUS COMMUNIS LEAVES EXTRACT: CHARACTERIZATTION, ANTIOXIDANT AND CATALYTIC ACTIVITY

被引:0
|
作者
Al-Jubouri, A. K. [1 ]
Al-Saadi, N. H. [1 ]
Kadhim, M. A. [1 ]
机构
[1] Univ Kerbala, Coll Sci, Dept Chem, Kerbala, Iraq
来源
关键词
nanoparticles; Myrtus communis; Plant extracts; catalytic activity;
D O I
暂无
中图分类号
S [农业科学];
学科分类号
09 ;
摘要
A simple, cost-effective, and environmentally friendly method for making green nanoparticles has been developed. The current study examines the use of M. communis leaves extract in the biosynthesis of copper nanoparticles (CuNPs). The color change and UV-visible spectrophotometer, which showed a distinct peak at 481nm, confirmed the formation of these particles. Different techniques were used to characterize copper nanoparticles. The influential functional groups that can bio-reduce the copper ion Cu2+ were identified using Fourier Transform Infrared (FT-IR) spectroscopy. The crystal structure of copper nanoparticles was determined using X-ray diffraction (XRD), as evidenced by the peaks at 2 theta values of 43.35, 50.50, and 74.21. In transmission electron microscopy (TEM), the particles have spherical morphology with an average diameter of 35-75 nm, while scanning electron microscopy (SEM) reveals the sphere-like shape of CuNPs. Copper-NPs synthesized in this study were tested as antioxidant and catalytic substances. CuNPs had superior radical scavenging activity when compared to an extract from Myrtus communis leaves. It is common to use 4-nitrophenol (4-NP) as a model reaction to evaluate synthesized nanomaterials' catalytic properties. borohydride (BH) was found to bind to the surface of CuNPs, indicating that it is an adsorbent. As the BH concentration increased, we observed a blue shift in the surface plasmon resonance (SPR) of CuNPs. These shifts increase in direct proportion to BH concentration, as does 4-NP to 4-amino phenol (4- AP) conversion. Accordingly, CuNPs have better catalytic activity than extract at higher BH concentrations
引用
收藏
页码:471 / 486
页数:16
相关论文
共 50 条
  • [1] ANTI-INFLAMMATORY AND ANTI- BACTERIAL ACTIVITY OF COPPER NANOPARTICLES SYNTHESIZED FROM MYRTUS COMMUNIS LEAVES EXTRACT
    Al-Jubouri, A. K.
    Al-Saadi, N. H.
    Kadhim, M. A.
    IRAQI JOURNAL OF AGRICULTURAL SCIENCES, 2022, 53 (03): : 698 - 711
  • [2] Green Synthesis of Silver Nanoparticles from Cassia Obtusifolia Leaves Extract: Characterization and Antioxidant Activity
    Flaih, Laheeb Subhy
    Al-Saadi, Narjis Hadi
    8TH INTERNATIONAL CONFERENCE ON APPLIED SCIENCE AND TECHNOLOGY (ICAST 2020), 2020, 2290
  • [3] Green synthesis of copper nanoparticles using Eclipta prostrata leaves extract and their antioxidant and cytotoxic activities
    Chung, Ill-Min
    Rahuman, Abdul Abdul
    Marimuthu, Sampath
    Kirthi, Arivarasan Vishnu
    Anbarasan, Karunanithi
    Padmini, Parthasarathy
    Rajakumar, Govindasamy
    EXPERIMENTAL AND THERAPEUTIC MEDICINE, 2017, 14 (01) : 18 - 24
  • [4] Antioxidant activity of the methanolic extract of Ricinus communis leaves
    Gupta, Mahesh Kumar
    Sharma, P. K.
    Singh, Ramesh
    Ansari, S. H.
    ASIAN JOURNAL OF CHEMISTRY, 2007, 19 (05) : 3387 - 3392
  • [5] Green synthesis of copper nanoparticles using Citrullus colocynthis leaves extract: photocatalytic, antimicrobial and antioxidant studies
    Nazir, Arif
    Alam, Shakeel
    Alwadai, Norah
    Abbas, Mazhar
    Bibi, Ismat
    Ali, Abid
    Ahmad, Naveed
    Al Huwayz, Maryam
    Iqbal, Munawar
    ZEITSCHRIFT FUR PHYSIKALISCHE CHEMIE-INTERNATIONAL JOURNAL OF RESEARCH IN PHYSICAL CHEMISTRY & CHEMICAL PHYSICS, 2023, 237 (11): : 1733 - 1751
  • [6] GREEN SYNTHESIS AND CHARACTERIZATION OF COPPER NANOPARTICLES DERIVED FROM MURRAYA KOENIGII LEAVES EXTRACT
    Sowmiya, K.
    Purushothaman, R.
    Shalini, Chinnadurai
    INTERNATIONAL JOURNAL OF LIFE SCIENCE AND PHARMA RESEARCH, 2021, : 220 - 224
  • [7] Reevaluation of bioactivity and antioxidant activity of Myrtus communis extract before and after encapsulation in liposomes
    Gortzi, Olga
    Lalas, Stavros
    Chinou, Ioanna
    Tsaknis, John
    EUROPEAN FOOD RESEARCH AND TECHNOLOGY, 2008, 226 (03) : 583 - 590
  • [8] Reevaluation of bioactivity and antioxidant activity of Myrtus communis extract before and after encapsulation in liposomes
    Olga Gortzi
    Stavros Lalas
    Ioanna Chinou
    John Tsaknis
    European Food Research and Technology, 2008, 226 : 583 - 590
  • [9] Radical scavenging activity and antioxidant activity of liquors of myrtle (Myrtus communis L.) berries and leaves
    Alamanni, MC
    Cossu, M
    ITALIAN JOURNAL OF FOOD SCIENCE, 2004, 16 (02) : 197 - 208
  • [10] Antioxidant activity of oligomeric acylphloroglucinols from Myrtus communis L.
    Rosa, A
    Deiana, M
    Casu, V
    Corona, G
    Appendino, G
    Bianchi, F
    Ballero, M
    Dessì, MA
    FREE RADICAL RESEARCH, 2003, 37 (09) : 1013 - 1019