The synthesis of novel polycyclic heterocyclic ring systems via photocyclization.: 20.: Benzo[h]thieno[3′,2′:4,5]thieno[2,3-c]quinoline, benzo[f]thieno[3′,2′:4,5]thieno[2,3-c]quinoline, benzo[f]thieno[3′,2′:4,5]thieno[2,3-c]tetrazolo[1,5-a]quinoline and benzo[f]thieno[3′,2′:4,5]thieno[2,3-c][1,2,4]triazolo[4,3-a]quinoline

被引：11
|
作者：
Luo, JK [1 ]
Federspiel, RF [1 ]
Castle, RN [1 ]
机构：
[1] Univ S Florida, Dept Chem, Tampa, FL 33620 USA
来源：
JOURNAL OF HETEROCYCLIC CHEMISTRY | 1998年 / 35卷 / 06期
关键词：
D O I：
10.1002/jhet.5570350637
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Four previously unknown polycyclic heterocyclic ring systems, namely, benzo[h]thieno[3',2':4, 5]thieno[2,3-c]quinoline (6), benzo[h]thieno[3',2':4,5]thieno[2,3-c]quinoline (11), benzo[f]thieno[3',2':4,5] thieno[2,3-c] tetrazolo[1,5-a]quinoline (12) and benzo[f]thieno [3',2':4,5] thieno[2,3-c][1,2,4] triazolo[4,3-a]quinoline (13), were synthesized via oxidative photocyclization. Unequivocal total assignments of the proton and carbon nmr spectra of 6 and 11 were made through the concerted usage of COSY, HMQC and HMBC two-dimensional nmr spectroscopic methods.
引用
收藏
页码：1441 / 1444
页数：4
相关论文
共 50 条
  • [21] THE SYNTHESIS OF MONOMETHOXYNAPHTHO[1',2'-4,5]THIENO[2,3-C]QUINOLINES
    PAKRAY, S
    CASTLE, RN
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1987, 24 (01) : 231 - 233
  • [22] Synthesis of Some Novel Thieno[2,3-c]pyridazines, Pyrimidothienopyridazines and Related Triazolo[1"5":1′,6′]pyrimido[4′,5′:4,5]thieno [2,3-c]pyridazines
    El-Dean, A. M. Kamal
    Al-Kamali, A. S. N.
    AFINIDAD, 2009, 66 (539) : 70 - 75
  • [23] Synthesis, photochemical synthesis and antitumor evaluation of novel derivatives of thieno[3′,2′:4,5]thieno[2,3-c]quinolones
    DoganKoruznjak, J
    Slade, N
    Zamola, B
    Pavelic, K
    Karminski-Zamola, G
    CHEMICAL & PHARMACEUTICAL BULLETIN, 2002, 50 (05) : 656 - 660
  • [24] SYNTHESIS OF PYRIDO[3',2'-4,5]THIENO[2,3-E]-1,2,4-TRIAZOLO[4,3-C]PYRIMIDINES AND THE ISOMERIC PYRIDO[3',2'-4,5]THIENO[2,3-E]-1,2,4-TRIAZOLO[2,3-C]PYRIMIDINES
    HILLER, K
    BADER, G
    REZNICEK, G
    JURENITSCH, J
    KUBELKA, W
    PHARMAZIE, 1991, 46 (06): : 405 - 408
  • [25] SYNTHESIS AND REACTIONS OF THIENO-[2'.3'-5.4]THIENO[2.3-C]PYRILIUM AND THIENOL[2',3'-4,5]THIENO[2,3-C]PYRILIUM SALTS
    DULENKO, VI
    TOLKUNOV, SV
    ALEKSEYEV, NN
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1983, (01): : 37 - 41
  • [26] Synthesis of pyrimido[4',5':4,5]thieno[2,3-c]pyridazine derivatives
    Quintela, JM
    Veiga, MC
    AlvarezSarandes, R
    Peinador, C
    MONATSHEFTE FUR CHEMIE, 1996, 127 (05): : 537 - 547
  • [27] A synthesis of new pyrido[2',3':4,5]thieno[2,3-c]pyridazine derivatives
    Veiga, MC
    Quintela, JM
    Peinador, C
    HETEROCYCLES, 1996, 43 (05) : 1073 - 1081
  • [28] Synthesis of pyrido[3′,2′:4,5]thieno[2,3-c]cinnolines - A new heterocyclic system
    Artemov V.A.
    Ivanov V.L.
    Koshkarov A.V.
    Shestopalov A.M.
    Litvinov V.P.
    Chemistry of Heterocyclic Compounds, 1998, 34 (1) : 96 - 101
  • [29] CONDENSED PYRIDINE BASES - SYNTHESIS OF SOME DERIVATIVES OF BENZO[B]FURO[2,3-C]QUINOLINE, BENZO[B]THIENO[2,3-C]QUINOLINE AND BENZO[B]SELENOPHENO[2,3-C]QUINOLINE
    TOLKUNOV, SV
    KHIZHAN, AI
    SIMONOVA, SI
    SEMENOV, NS
    LYASHCHUK, SN
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1994, (03): : 321 - 326
  • [30] Fused quinoline heterocycles VII: synthesis of new isoxazolo[3′,4′:4,5]pyrrolo(or thieno)[2,3-c]quinolines
    Mekheimer, Ramadan A.
    Hameed, Afaf M. Abdel
    Sadek, Kamal U.
    ARKIVOC, 2008, : 144 - 153
12345