Microwave-assisted polyol synthesis of CulnTe2 and CulnSe2 nanoparticles

被引:126
作者
Grisaru, H
Palchik, O
Gedanken, A [1 ]
Palchik, V
Slifkin, MA
Weiss, AM
机构
[1] Bar Ilan Univ, Dept Chem, IL-52900 Ramat Gan, Israel
[2] Jerusalem Coll Technol, Dept Elect, IL-91160 Jerusalem, Israel
关键词
D O I
10.1021/ic0342853
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Nanoparticles of the CuInTe2 (CIT) and CuInSe2 (CIS) alloys have been prepared using the microwave-assisted polyol method. In this simple and quick reaction the polyol is both the solvent and the reducing agent. XRD studies show that nanoparticles of CIT and CIS are formed in the body-centered tetragonal structure and their average diameters are similar to94 and similar to83 nm, respectively. Electron microscopy studies show that these formed particles are poorly aggregated with a mean diameter of 100 and 85 nm, respectively. The products have been characterized by different analytical techniques, and the electronic properties have been measured using photoacoustic spectroscopy (PAS).
引用
收藏
页码:7148 / 7155
页数:8
相关论文
共 48 条
  • [1] Electrodeposition of CuInSe2 thin films and their characteristics
    Al-Bassam, AAI
    [J]. PHYSICA B, 1999, 266 (03): : 192 - 197
  • [2] Material properties and growth mechanism of CuInSe2 prepared by H2Se treatment of metallic alloys
    Alberts, V
    Schon, JH
    Bucher, E
    [J]. JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 1999, 10 (07) : 469 - 474
  • [3] [Anonymous], 1980, Photoacoustics and Photoacoustic Spectroscopy
  • [4] Low cost techniques for the preparation of Cu(In,Ga)(Se,S)2 absorber layers
    Basol, BM
    [J]. THIN SOLID FILMS, 2000, 361 : 514 - 519
  • [5] BLIN B, 1989, NEW J CHEM, V13, P67
  • [6] Electrochemical reduction of noble metal compounds in ethylene glycol
    Bonet, F
    Guéry, C
    Guyomard, D
    Urbina, RH
    Tekaia-Elhsissen, K
    Tarascon, JM
    [J]. INTERNATIONAL JOURNAL OF INORGANIC MATERIALS, 1999, 1 (01): : 47 - 51
  • [7] Alternative approach to electroless Cu metallization of AlN by a nonaqueous polyol process
    Chow, GM
    Kurihara, LK
    Ma, D
    Feng, CR
    Schoen, PE
    MartinezMiranda, LJ
    [J]. APPLIED PHYSICS LETTERS, 1997, 70 (17) : 2315 - 2317
  • [8] Electrodeposition and characterisation of CuInSe2 for applications in thin film solar cells
    De Silva, KTL
    Priyantha, WAA
    Jayanetti, JKDS
    Chithrani, BD
    Siripala, W
    Blake, K
    Dharmadasa, IM
    [J]. THIN SOLID FILMS, 2001, 382 (1-2) : 158 - 163
  • [9] SOLID-STATE CHEMISTRY - A REDISCOVERED CHEMICAL FRONTIER
    DISALVO, FJ
    [J]. SCIENCE, 1990, 247 (4943) : 649 - 655
  • [10] Characterization of CuInTe2 thin films prepared by pulsed laser deposition
    Gremenok, VF
    Victorov, IA
    Bodnar, IV
    Hill, AE
    Pilkington, RD
    Tomlinson, RD
    Yakushev, MV
    [J]. MATERIALS LETTERS, 1998, 35 (1-2) : 130 - 134