Multicomponent reactions of ammonium thiocyanate, acyl chlorides, alkyl bromides, and enaminones: A facile one-pot synthesis of thiophenes

被引：13

作者：

Hossaini, Zinatossadat ^{[1
]}

Rostami-Charati, Faramarz ^{[2
]}

Soltani, Samira ^{[1
]}

Mirzaei, Anwar ^{[3
]}

Berijani, Kayhaneh ^{[1
]}

机构：

[1] Islamic Azad Univ, Dept Chem, Qaemshahr Branch, Qaemshahr, Iran

[2] Gonbad Kavous Univ, Dept Chem, Fac Sci, Gonbad, Iran

[3] Islamic Azad Univ, Dept Chem, Sanandaj Branch, Sanandaj, Iran

来源：

MOLECULAR DIVERSITY | 2011年 / 15卷 / 04期

关键词：

Thiophene; Ammonium thiocyanate; Carbonyl compounds; Solvent-free conditions; SUBSTITUTED THIOPHENES;

D O I：

10.1007/s11030-011-9322-5

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

An efficient synthesis of thiophene derivatives is described via one-pot reaction between ammonium thiocyanate, acyl chlorides, alpha-halocarbonyls, and enaminones under solvent-free conditions at 65 degrees C. The mild reaction conditions and high yields of the products exhibit the good synthetic advantage of these methods.

引用

页码：911 / 916

页数：6

共 21 条

[1] Multicomponent reactions of ammonium thiocyanate, acyl chlorides, alkyl bromides, and enaminones: A facile one-pot synthesis of thiophenes
Zinatossadat Hossaini
Faramarz Rostami-Charati
Samira Soltani
Anwar Mirzaei
Kayhaneh Berijani
Molecular Diversity, 2011, 15 : 911 - 916
[2] A one-pot synthesis of alkyl acylcarbamodithioates from acid chlorides, thiols, and ammonium thiocyanate
Yavari, Issa
Iravani, Nasir
Sayyed-Alangi, S. Zahra
Hajinasiri, Rahimeh
MONATSHEFTE FUR CHEMIE, 2009, 140 (10): : 1199 - 1204
[3] A one-pot synthesis of alkyl acylcarbamodithioates from acid chlorides, thiols, and ammonium thiocyanate
Issa Yavari
Nasir Iravani
S. Zahra Sayyed-Alangi
Rahimeh Hajinasiri
Monatshefte für Chemie - Chemical Monthly, 2009, 140 : 1199 - 1204
[4] A one-pot multicomponent synthesis of polysubstituted thiophenes via the reactions of an isocyanide, α-haloketones, and β-ketodithioesters in water
Moghaddam, Firouz MatIoubi
Khodabakhshi, Mohammad Reza
Latifkar, Arash
TETRAHEDRON LETTERS, 2014, 55 (06) : 1251 - 1254
[5] An efficient one-pot synthesis of tri-substituted thiophenes via a multicomponent reaction in water
Moghaddam, Firouz Matloubi
Bardajee, Ghasem Rezanejade
Dolabi, Maliheh
JOURNAL OF SULFUR CHEMISTRY, 2010, 31 (05) : 387 - 393
[6] A Mild and Facile One-Pot Synthesis of N-Methyl-3-Acyl-Pyrroles
Valizadeh, Hassan
Fakhari, Ashraf
MOLECULES, 2010, 15 (05) : 2972 - 2979
[7] Four-component one-pot synthesis of functionalized ynamines from reaction of benzoyl chlorides, secondary amines, acetylenic esters and ammonium thiocyanate
Yavari, Issa
Sabbaghan, Maryam
Hosseim, Nargess
Hossaini, Zinatossadat
SYNLETT, 2007, (20) : 3172 - 3174
[8] One-pot synthesis of 1-methylimidazol-2-yl N-aroyldithiocarbamates from 2-mercapto-1-methylimidazole, ammonium thiocyanate and aroyl chlorides
Dehvari, Fatemeh
Hassanabadi, Alireza
JOURNAL OF CHEMICAL RESEARCH, 2015, (08) : 462 - 463
[9] Synthesis of homoallylic amines and acylhydrazides by tin powder-promoted multicomponent one-pot allylation reactions
Ma, Junyan
Huang, Danfeng
Wang, Ke-Hu
Xu, Yanli
Chong, Siying
Su, Yingpeng
Fu, Ying
Hu, Yulai
APPLIED ORGANOMETALLIC CHEMISTRY, 2016, 30 (07) : 571 - 576
[10] A Straightforward and Efficient Catalyst-free One-pot Synthesis of N-Acyl-1,3-diary1-2-azaphenalene Derivatives via Multicomponent Reactions
Foroughifar, Naser
Mobinikhaledi, Akbar
Moghanian, Hassan
CHEMISTRY LETTERS, 2010, 39 (03) : 180 - 181

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