Ultra-turrax based ultrasound-assisted extraction of five organic acids from honeysuckle (Lonicera japonica Thunb.) and optimization of extraction process

被引：45
作者：
Xu, Wen-Jing [1 ,2 ]
Zhai, Jia-Wen [1 ,2 ]
Cui, Qi [1 ,2 ]
Liu, Ju-Zhao [1 ,2 ]
Luo, Meng [1 ,2 ]
Fu, Yu-Jie [1 ,2 ,3 ]
Zu, Yuan-Gang [1 ,2 ]
机构：
[1] Northeast Forestry Univ, Key Lab Forest Plant Ecol, Minist Educ, Harbin 150040, Peoples R China
[2] Northeast Forestry Univ, Engn Res Ctr Forest Biopreparat, Minist Educ, Harbin 150040, Peoples R China
[3] Northeast Forestry Univ, Collaborat Innovat Ctr Dev & Utilizat Forest Reso, Harbin 150040, Peoples R China
来源：
SEPARATION AND PURIFICATION TECHNOLOGY | 2016年 / 166卷
基金：
中国国家自然科学基金;
关键词：
Honeysuckle; Ultra-turrax based ultrasound-assisted extraction; Mass transfer kinetics; Particle size distribution; PRESSURE CAVITATION EXTRACTION; PHENOLIC-COMPOUNDS; CHLOROGENIC ACID; ROTOR-STATOR; SEPARATION; CONSTITUENTS; FLAVONOIDS; ROOTS; TIME;
D O I：
10.1016/j.seppur.2016.04.003
中图分类号：
TQ [化学工业];
学科分类号：
0817 ;
摘要：
In the present study, a highly effective extraction method, namely ultra-turrax based ultrasound-assisted extraction (UT-UAE), was firstly designed to extract the main organic acids from honeysuckle. Single factor experiments and Box-Behnken design (BBD) were conducted to optimize the extraction process. The optimal extraction conditions were as follows: homogeneous rate 8000 rpm, ultrasonic intensity 0.347 W/cm(2), ethanol concentration 65%, time 10 min and liquid/solid ratio 20:1 mL/g. Moreover, the mass transfer kinetics and particle size distribution were investigated in order to demonstrate the advantages of UT-UAE. Through the comparison with ultra-turrax extraction (UTE) and ultrasound-assisted extraction (UAE) methods, the proposed method exhibited higher yields of five target organic acids in a shorter time. The results showed that UT-UAE could be a promising method for fast extracting active compounds from plants. (C) 2016 Elsevier B.V. All rights reserved.
引用
收藏
页码：73 / 82
页数：10
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