Synthesis of Co3O4 nanoparticles via an ionic liquid-assisted methodology at room temperature

被引：86

作者：

Zou, Dingbing ^{[1
]}

Xu, Chao ^{[1
]}

Luo, Hao ^{[1
]}

Wang, Ling ^{[1
]}

Ying, Taokai ^{[1
,2
]}

机构：

[1] Zhejiang Normal Univ, Coll Chem & Life Sci, Jinhua 321004, Peoples R China

[2] Zhejiang Normal Univ, Inst Phys Chem, Jinhua 321004, Peoples R China

来源：

MATERIALS LETTERS | 2008年 / 62卷 / 12-13期

关键词：

Co3O4; ionic liquids; nanomaterials; semiconductors;

D O I：

10.1016/j.matlet.2007.10.056

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Cobalt oxide (Co3O4) nanoparticles have been successfully synthesized through a facile solution oxidation route at room temperature and normal pressure for 6h at first time, using an ionic liquid 1-n-butyl-3-methylimidazolium hydroxide ([BMIM]OH) as an assisted agent and electrical conductor. The structure and morphology of as-prepared Co3O4 nanoparticles were characterized by powder X-ray diffraction (XRD), infrared spectrum (IR), and scanning electron microscope (SEM). XRD studies indicated that the product was well-crystallized cubic phase of Co3O4 with a cell constant of a = 8.0722 angstrom. The SEM images showed that the obtained Co3O4 powders consisted of dispersive quasi-spherical particles with the size ranged from 10 to 50nm. The possible formation mechanism Of Co3O4 nanoparticles was simply proposed as well. (c) 2007 Elsevier B.V. All rights reserved.

引用

页码：1976 / 1978

页数：3

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