Synthesis and thermal behavior of the hydrogen praseodymium diphosphate (HPrP2O7•3H2O)

被引:7
|
作者
Chehimi-Moumen, F
Ben Hassen-Chehimi, D
Ferid, M
Trabelsi-Ayadi, M [1 ]
机构
[1] Fac Sci Bizerte, Lab Physicochim Minerale, Zarzouna Bizerte 7021, Tunisia
[2] Inst Natl Rech Sci & Tech, Lab Proc Chim, Hammam Lif 2050, Tunisia
来源
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY | 2001年 / 65卷 / 01期
关键词
chemical synthesis; diphosphate; infrared spectroscopy; thermogravimetric analysis; X-ray diffraction;
D O I
10.1023/A:1011520417067
中图分类号
O414.1 [热力学];
学科分类号
摘要
The preparation of a new acid lanthanide diphosphate is reported. The acid praseodymium diphosphate, obtained as a trihydrate salt, is investigated by chemical analysis, X-ray powder diffraction and IR spectroscopy. The study of the thermal behavior of HPrP2O7. 3H(2)O shows that its dehydration begins at 367 K. A scheme of its decomposition is proposed.
引用
收藏
页码:87 / 92
页数:6
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