Large-scale synthesis and radiolabelling of 6-deoxy-6-iodo-D-glucose (6-DIG)

被引：6

作者：

Charronneau, E

Mathieu, JP

Morin, C ^{[1
]}

机构：

[1] Univ Grenoble, Dept Chim, LEDSS, F-38402 St Martin Dheres, France

[2] Univ Grenoble, Dept Biophys, LER, F-38700 La Tronche, France

来源：

APPLIED RADIATION AND ISOTOPES | 1998年 / 49卷 / 12期

关键词：

D O I：

10.1016/S0969-8043(97)10142-7

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Multigram quantities of 6-deoxy-6-iodo-D-glucose (6-DIG) are conveniently obtained from its beta-peracetate; its radiolabelling has been performed by isotopic exchange. (C) 1998 Elsevier Science Ltd. All rights reserved.

引用

页码：1605 / 1607

页数：3

共 20 条

[1]

AKAGI M, 1963, CHEM PHARM BULL, V11, P559

[2] SYNTHESIS OF DEOXYHALOGENO SUGARS - REACTION OF HALIDE-IONS WITH 1,2,3,4-TETRA-O-ACETYL-6-O-[(TRIFLUOROMETHYL)SULFONYL]-BETA-D-GLUCOPYRANOSE [J].

AMBROSE, MG ;

BINKLEY, RW .

JOURNAL OF ORGANIC CHEMISTRY, 1983, 48 (05) :674-677

[3]

BIGNAN G, 1995, Patent No. 9634872

[4]

BIGNAN G, 1995, Patent No. 95214

[5] NEW HALOGENATION REAGENT SYSTEMS USEFUL FOR THE MILD ONE-STEP CONVERSION OF ALCOHOLS INTO IODIDES OR BROMIDES [J].

CLASSON, B ;

LIU, ZC ;

SAMUELSSON, B .

JOURNAL OF ORGANIC CHEMISTRY, 1988, 53 (26) :6126-6130

[6] DIFRUCTOSE DIANHYDRIDES FROM SUCROSE AND FRUCTOOLIGOSACCHARIDES AND THEIR USE AS BUILDING-BLOCKS FOR THE PREPARATION OF AMPHIPHILES, LIQUID-CRYSTALS, AND POLYMERS [J].

FERNANDEZ, JMG ;

GADELLE, A ;

DEFAYE, J .

CARBOHYDRATE RESEARCH, 1994, 265 (02) :249-269

[7] IODINE-123-LABELED GLUCOSE ANALOGS - PROSPECTS FOR A SINGLE-PHOTON-EMITTING ANALOG OF FLUORINE-18-LABELED DEOXYGLUCOSE [J].

GATLEY, SJ .

NUCLEAR MEDICINE AND BIOLOGY, 1995, 22 (07) :829-835

[8] THE BETA-IODOETHOXYL GROUP - A STABLE UNIT FOR RADIOIODINATION [J].

HAMANT, S ;

MATHIEU, JP ;

MORIN, C ;

TRIMCEV, I ;

VIDAL, M .

BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 1994, 4 (14) :1687-1690

[9] *UBER DIE HERSTELLUNG VON ALPHA-CHINOVOSE-TETRAACETAT UND BETA-CHINOVOSE-TETRAACETAT AUS GLUCOSE [J].

HARDEGGER, E ;

MONTAVON, RM .

HELVETICA CHIMICA ACTA, 1946, 29 (05) :1199-1203

[10]

HELFERICH B, 1928, CHEM BERICHTE DTSCH, V61, P1640

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