Ethyl [(benzylazaniumyl)(2-hydroxyphenyl)methyl]phosphonate

被引:0
作者
Zhang, Xiangdong [1 ]
Zhang, Rui [1 ]
Ge, Chunhua [1 ]
Zhang, Xiaoyan [1 ]
机构
[1] Liaoning Univ, Coll Chem, Shenyang 110036, Liaoning, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
基金
中国国家自然科学基金;
关键词
data-to-parameter ratio = 14.9; mean σ(CC) = 0.005 Å; R factor = 0.049; single-crystal X-ray study; T = 296 K; wR factor = 0.121;
D O I
10.1107/S1600536811026444
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C16H20NO4P, crystallizes as a zwitterion. In the molecule, the two aromatic rings form a dihedral angle of 55.2 (1)degrees. In the crystal, intermolecular N-H center dot center dot center dot O and O-H center dot center dot center dot O hydrogen bonds link the molecules into columns propagating in [010].
引用
收藏
页码:O2006 / U253
页数:8
相关论文
共 6 条
[1]  
Bruker AXS Inc, 2001, SMART SAINT SADABS
[2]  
Farrugia L. J., 1999, Journal of Applied Crystallography, V32, P837, DOI [DOI 10.1107/S0021889812029111, 10.1107/S0021889899006020, DOI 10.1107/S0021889899006020]
[3]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[4]   Structure validation in chemical crystallography [J].
Spek, Anthony L. .
ACTA CRYSTALLOGRAPHICA SECTION D-STRUCTURAL BIOLOGY, 2009, 65 :148-155
[5]   Ethyl [(2-hydroxyethylaminio)(2-hydroxyphenyl) methyl]phosphonate dihydrate [J].
Zhang, XD ;
Yu, Z ;
Ma, YC ;
Zhao, Z ;
Zhu, ML .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O2952-O2954
[6]   Ethyl [(n-butylammonio)(2-hydroxyphenyl)methyl]phosphonate [J].
Zhang, Xiaoyan ;
Ge, Chunhua ;
Zhang, Xiangdong ;
Liu, Qitao .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 :O4778-U5685