Pore size analysis of mesoporous films by krypton adsorption

被引:0
作者
Chao, K [1 ]
Ping, H
Chiu, C
Chiang, AST
机构
[1] Natl Tsing Hua Univ, Dept Chem, Hsinchu, Taiwan
[2] Natl Cent Univ, Dept Chem & Mat Engn, Chungli 32054, Taiwan
来源
RECENT ADVANCES IN THE SCIENCE AND TECHNOLOGY OF ZEOLITES AND RELATED MATERIALS, PTS A - C | 2004年 / 154卷
关键词
krypton adsorption; mesoporous film; pore size analysis;
D O I
暂无
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The pore structure of mesoporous membranes coated oil silicon wafer was characterized by the adsorption of krypton at 77 K ill this Study. To establish the capillary condensation and evaporation conditions for krypton at this temperature, the adsorption of both nitrogen and krypton were first measured oil a series of Siliceous MCM-41, MCM-48 and SBA-15 reference samples. The adsorption and desorption transition of krypton were then correlated with the pore size deduced from the nitrogen isotherm. Finally, the obtained correlation was applied to estimate the pore size distribution of niesoporous films.
引用
收藏
页码:1363 / 1368
页数:6
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