Efficient sonochemical green reaction of aldehyde, thiobarbituric acid and ammonium acetate using magnetically recyclable nanocatalyst in water

被引：38

作者：

Naeimi, Hossein ^{[1
]}

Didar, Asieh ^{[1
]}

机构：

[1] Univ Kashan, Dept Organ Chem, Fac Chem, Kashan 87317, Iran

来源：

ULTRASONICS SONOCHEMISTRY | 2017年 / 34卷

关键词：

Ultrasound; Dipyrimidine; Magnetic; Aldehyde; 2-Thiobarbituric acid; GEM-DICHLOROAZIRIDINE DERIVATIVES; ONE-POT; HETEROGENEOUS CATALYST; ANTIINFLAMMATORY AGENTS; 3-COMPONENT SYNTHESIS; ASSISTED SYNTHESIS; AQUEOUS-MEDIUM; NANOPARTICLES; ULTRASOUND; CUFE2O4;

D O I：

10.1016/j.ultsonch.2016.07.021

中图分类号：

O42 [声学];

学科分类号：

070206 ; 082403 ;

摘要：

A facile one-pot and four-component economical synthesis of pyrido[2,3-d:6,5-d]dipyrimidines using aldehyde, 2-thiobarbituric acid and ammonium acetate in the presence of magnetically heterogeneous catalyst under ultrasonic irradiation in water is described. The present synthesis shows attractive characteristics such as; the use of magnetically recoverable and reusable catalyst, convenient one-pot operation, short reaction periods, high to excellent yields and the use of water as a green reaction medium, mild reaction conditions and is considered to be relatively environmentally benign. (C) 2016 Elsevier B.V. All rights reserved.

引用

页码：889 / 895

页数：7

共 42 条

[1] Abdulla R.F., 1988, Aldrichimica Acta, V21, P31
[2] PYRIDO[2,3-D]PYRIMIDINES .4. SYNTHETIC STUDIES LEADING TO VARIOUS OXOPYRIDO[2,3-D]PYRIMIDINES
BROOM, AD
SHIM, JL
ANDERSON, GL
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1976, 41 (07) : 1095 - 1099
[3] Bystryakova I.D., 1991, J PHARM CHEM, V25, P874, DOI [10.1007/BF00778976, DOI 10.1007/BF00778976]
[4] Discovery and structure-activity studies of a novel series of pyrido[2,3-d]pyrimidine tyrosine kinase inhibitors
Connolly, CJC
Hamby, JM
Schroeder, MC
Barvian, M
Lu, GH
Panek, RL
Amar, A
Shen, C
Kraker, AJ
Fry, DW
Klohs, WD
Doherty, AM
[J]. BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 1997, 7 (18) : 2415 - 2420
[5] Corre L.L., 2010, ORG BIOMOL CHEM, V8, P2164
[6] Power ultrasound in organic systhesis: moving cavitational chemistry from academia to innovative and large-scale applications
Cravotto, G
Cintas, P
[J]. CHEMICAL SOCIETY REVIEWS, 2006, 35 (02) : 180 - 196
[7] One-Pot, Three-Component Synthesis of a Library of Spirooxindole-Pyrimidines Catalyzed by Magnetic Nanoparticle Supported Dodecyl Benzenesulfonic Acid in Aqueous Media
Deng, Jia
Mo, Li-Ping
Zhao, Fei-Yang
Zhang, Zhan-Hui
Liu, Shou-Xin
[J]. ACS COMBINATORIAL SCIENCE, 2012, 14 (05) : 335 - 341
[8] Deyanov AB, 1991, J PHARM CHEM, V25, P248, DOI DOI 10.1007/BF00772106
[9] SYNTHESIS AND ANTIMICROBIAL ACTIVITY OF 6,7-ANNULATED PYRIDO[2,3-D]PYRIMIDINES
DONKOR, IO
KLEIN, CL
LIANG, L
ZHU, NJ
BRADLEY, E
CLARK, AM
[J]. JOURNAL OF PHARMACEUTICAL SCIENCES, 1995, 84 (05) : 661 - 664
[10] Synthesis of 4-substituted pyrido[2,3-d]pyrimidin-4(1H)-one as analgesic and anti-inflammatory agents
El-Gazzar, Abdel-Rahman B. A.
Hafez, Hend N.
[J]. BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2009, 19 (13) : 3392 - 3397

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