N-(2-chloro-2-nitro-1-phenylpropyl)-4-methylbenzenesulfonamide

被引:2
作者
Zhi, Sanjun [1 ]
Li, Tengfei [1 ]
An, Guanghui [1 ]
Pan, Yi [1 ]
机构
[1] Nanjing Univ, Sch Chem & Chem Engn, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷
关键词
D O I
10.1107/S1600536807067712
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C16H17ClN2O4S, the dihedral angle between the phenyl and benzene rings is 19.4 (2)degrees. The crystal packing is stabilized by intermolecular N-H center dot center dot center dot O hydrogen bonds, as well as by intra- and intermolecular C-H center dot center dot center dot O hydrogen bonds.
引用
收藏
页码:O357 / U1586
页数:9
相关论文
共 11 条
[1]   TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].
ALLEN, FH ;
KENNARD, O ;
WATSON, DG ;
BRAMMER, L ;
ORPEN, AG ;
TAYLOR, R .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19
[2]  
*BRUK AXS INC, 2000, SADABS VERS 2 0 3
[3]  
*BRUK AXS INC, 2000, SAINT VERS 6 0 1
[4]  
*BRUK AXS INC, 2000, SMART VERS 5 6 2 5
[5]  
*BRUK AXS INC, 2000, SHELXTL VERS 6 1 0
[6]   CuCl-catalyzed regio- and stereoselective aminohalogenation of α,β-unsaturated nitriles [J].
Han, Jian-Lin ;
Zhi, San-Jun ;
Wang, Le-Yong ;
Pan, Yi ;
Li, Guigen .
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2007, 2007 (08) :1332-1337
[7]  
Kemp J. E. G., 1991, COMPREHENSIVE ORGANI, V3, P469
[8]   Recent development of regio- and stereoselective aminohalogenation reaction of alkenes [J].
Li, Guigen ;
Kotti, S. R. S. Saibabu ;
Timmons, Cody .
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2007, 2007 (17) :2745-2758
[9]   STEREOSELECTIVE SYNTHESIS OF PROTECTED AMINES AND DIAMINES FROM ALKENES USING N,N-DICHLORO-TERT-BUTYLCARBAMATE [J].
ORLEK, BS ;
STEMP, G .
TETRAHEDRON LETTERS, 1991, 32 (32) :4045-4048
[10]  
Qui J., 2000, J MED CHEM, V43, P706