DEVELOPMENT AND VALIDATION OF A RAPID AND ENVIRONMENTALLY FRIENDLY ANALYSIS METHOD FOR DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS IN WATER BY MODIFICATION OF QuEChERS EXTRACTION METHOD

被引：0

作者：

Sik, B. ^{[1
]}

Tongur, T. ^{[1
]}

Erkaymaz, T. ^{[1
]}

Yatmaz, H. A. ^{[1
]}

机构：

[1] Akdeniz Univ, Food Safety & Agr Res Ctr, Antalya, Turkey

来源：

JOURNAL OF ENVIRONMENTAL PROTECTION AND ECOLOGY | 2016年 / 17卷 / 02期

关键词：

PAH; water; analysis; method development; contamination; SAMPLE PREPARATION; SURFACE WATERS; PAHS; GC/MS; MS;

D O I：

暂无

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

In this study a rapid and environmentally friendly analysis method for the determination of 16 polycyclic aromatic hydrocarbon compounds (PAHs) in water was developed and validated. Water samples were extracted by modified QuEChERS method and analysed by gas chromatography mass spectrometer (GC-MS). Analytical separation was achieved in 18 min. The calibration curves were linear in the selected range of each analyte. Limit of detections of PAHs were between 0.16 and 0.31 mu g kg(-1) % Recovery, repeatability (RSDr) and reproducibility (RSDR) values met AOAC method validation acceptance criteria.

引用

页码：435 / 444

页数：10

共 24 条

[1] QuEChERS Method for the Determination of PAH Compounds in Sardinia Sea Urchin (Paracentrotus lividus) Roe, Using Gas Chromatography ITMS-MS Analysis [J].

Angioni, Alberto ;

Porcu, Luciano ;

Secci, Marco ;

Addis, Pierantonio .

FOOD ANALYTICAL METHODS, 2012, 5 (05) :1131-1136

[2]

*AOAC INT, 2002, AOAC GUID SINGL LAB

[3]

AOAC Official Methods of Analysis, 2012, AOAC OFFICIAL METHOD

[4] Multi-residue analysis and ultra-trace quantification of 36 priority substances from the European Water Framework Directive by GC-MS and LC-FLD-MS/MS in surface waters [J].

Barrek, Sami ;

Cren-Olive, Cecile ;

Wiest, Laure ;

Baudot, Robert ;

Arnaudguilhem, Carine ;

Grenier-Loustalot, Marie-Florence .

TALANTA, 2009, 79 (03) :712-722

[5] Analysis of polycyclic aromatic hydrocarbons (PAHs) in airborne particles by direct sample introduction thermal desorption GC/MS [J].

Bates, Matthew ;

Bruno, Paolo ;

Caputi, Mariangela ;

Caselli, Maurizio ;

de Gennaro, Gianluigi ;

Tutino, Maria .

ATMOSPHERIC ENVIRONMENT, 2008, 42 (24) :6144-6151

[6] Optimisation of pressurised liquid extraction for the ultra-trace quantification of 20 priority substances from the European Water Framework Directive in atmospheric particles by GC-MS and LC-FLD-MS/MS [J].

Becouze, Celine ;

Wiest, Laure ;

Baudot, Robert ;

Bertrand-Krajewski, Jean-Luc ;

Cren-Olive, Cecile .

ANALYTICA CHIMICA ACTA, 2011, 693 (1-2) :47-53

[7]

Bispo J.R. L., 2011, AM J ANAL CHEM, V2, P971, DOI [DOI 10.4236/AJAC2011.28113, 10.1016/j.microc.2006.06.002, DOI 10.1016/J.MICROC.2006.06.002]

[8] Distributions of polycyclic aromatic hydrocarbons in surface waters, sediments and soils of Hangzhou City, China [J].

Chen, BL ;

Xuan, XD ;

Zhu, LZ ;

Wang, J ;

Gao, YZ ;

Yang, K ;

Shen, XY ;

Lou, BF .

WATER RESEARCH, 2004, 38 (16) :3558-3568

[9]

Crompton T.R., 2002, DETERMINATION ORGANI

[10]

European Union (EU), 2006, OFF J EUR UNION L, V215, P4

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