Fused deposition modeling of Si3N4 ceramics: A cost-effective 3D-printing route for dense and high performance non-oxide ceramic materials

被引:26
作者
Niu, Furong [1 ]
Yang, Xiaole [2 ]
Li, Yuanbing [2 ]
Guo, Jinyu [1 ]
Peng, Liu [1 ]
Xie, Zhipeng [3 ]
Yang, Xianfeng [1 ]
机构
[1] Changsha Univ Sci & Technol, Coll Mat Sci & Engn, Changsha 410014, Peoples R China
[2] Wuhan Univ Sci & Technol, State Key Lab Refractories & Met, Wuhan 430080, Peoples R China
[3] Tsinghua Univ, China State Key Lab New Ceram & Fine Proc, Beijing 100084, Peoples R China
基金
中国国家自然科学基金;
关键词
Fused deposition modeling; 3D printing; Silicon nitride; Additive manufacturing; ZIRCONIA CERAMICS; ALUMINA CERAMICS; FABRICATION; STRATEGY; POWDER; SLURRY;
D O I
10.1016/j.jeurceramsoc.2022.08.041
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Dense Si3N4 ceramics were prepared by fused deposition molding method accompanied by gas pressure sintering. In this study, the surface steps, inter layer bonding and microstructure evolution were characterized and dense Si3N4 ceramics without obvious defects were obtained. It was verified that layer thickness and nozzle diameter have little impact on the density and flexural strength of both green and sintered parts. As to the filling strategy, contour offset path was more effective to obtain sintered part with higher flexural strength than parallel lines and grid path, which was due to the possible voids appeared at the intersection of print paths with different di-rections. The highest flexure strength 824.74 +/- 85 MPa was obtained with layer thickness 0.15 mm, nozzle size 0.6 mm and contour offset path. The reliability of the obtained Si3N4 ceramics was also investigated and complex shaped Si3N4 ceramic parts with good shape keeping was prepared successfully.
引用
收藏
页码:7369 / 7376
页数:8
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