Development of an Automated Heavy Metal Analyser

被引：6

作者：

Cases-Utrera, Joana ^{[1
]}

Escude-Pujol, Roger ^{[1
]}

Ibanez-Otazua, Nora ^{[2
]}

Javier del Campo, F. ^{[1
]}

机构：

[1] Univ Autonoma Barcelona, IMB CNM CSIC, Inst Microelect Barcelona, E-08193 Barcelona, Spain

[2] Inkoa Inkoa Sistemas SL, Ribera Axpe, Dept 208, Erandio 48950, Bizkaia, Spain

来源：

ELECTROANALYSIS | 2015年 / 27卷 / 04期

关键词：

Automated analyzer; Heavy metals; Stripping voltammetry; Electrochemical instrumentation; Prototyping; ANODIC-STRIPPING VOLTAMMETRY; ZINC; BISMUTH; COPPER; LEAD; CADMIUM; FILM; FLOW; TRACE; MECHANISMS;

D O I：

10.1002/elan.201400614

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

This article describes the design, fabrication and characterization of a compact and deployable heavy metal analyzer. The system is autonomous and its micro-controller enables the configuration of its four micropumps and the application of different electroanalytical techniques. A range of prototyping and manufacturing techniques have been used in the fabrication of the instrument, including laser sintering, milling, and laser engraving. We present the electrochemical characterization of the system, and provide preliminary results obtained in the determination of Cu and Zn in different waters. The only sample treatment consists in its 1 : 2 dilution in pH 5.6 acetate buffer. Detection limits of 2.2 and 3.8 ppb were found for Cu and Zn, respectively.

引用

页码：929 / 937

页数：9

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