N2,N2′-Bis(3-nitrobenzylidene) pyridine-2,6-dicarbohydrazide dimethylformamide disolvate trihydrate

被引：2

作者：

Cheng, Cuixia ^{[1
]}

Liu, Haowen ^{[1
]}

机构：

[1] S Cent Univ Natl, Coll Chem & Mat Sci, Key Lab Catalysis & Mat Sci Hubei Provence, Wuhan 430074, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷

关键词：

D O I：

10.1107/S1600536807056607

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C21H15N7O6 center dot 2C(3)H(7)NO center dot 3H(2)O, the N-2,N-2'-bis(3-nitrobenzylidene)pyridine-2,6-dicarbohydrazide and one water molecule are located on a twofold rotation axis. The molecules are connected by hydrogen bonds. One dimethylformamide molecule is disordered over two positions; the site occupancy factors are ca 0.8 and 0.2.

引用

页码：O155 / U3901

页数：10

共 7 条

[1]

*BRUK AXS INC, 2001, SAINT PLUS VERS 6 45

[2] Synthesis and spectroscopic studies of trinuclear uranyl complexes with compartmental ligands H(4)L derived from 2,6-dipicolinoyl-hydrazine and 4-acyl-1-phenyl-3-methyl-pyrazolones-5 (where acyl equals benzoyl, acetyl, iso-butyryl or iso-valeroyl) [J].

Chen, XY ;

Zhan, SZ ;

Meng, QJ .

TRANSITION METAL CHEMISTRY, 1996, 21 (04) :345-348

[3] Synthesis, electrochemical and magnetic properties of Cu-3 complexes of a series of new compartmental trinucleating ligands H(4)L [J].

Chen, XY ;

Zhan, SZ ;

Hu, CJ ;

Meng, QJ ;

Liu, YJ .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1997, (02) :245-250

[4] COMPARTMENTAL LIGANDS - SYNTHESIS AND CHARACTERIZATION OF POLYNUCLEAR URANYL COMPLEXES [J].

PAOLUCCI, G ;

STELLUTO, S ;

SITRAN, S .

INORGANICA CHIMICA ACTA-F-BLOCK ELEMENTS ARTICLES AND LETTERS, 1985, 110 (01) :19-23

[5]

Sheldrick G. M., 2001, SADABS

[6]

Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR, P38

[7] Single-crystal structure validation with the program PLATON [J].

Spek, AL .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :7-13

← 1 →