Synthesis and characterizations of nano sized MgO and its nano composite with poly(vinyl alcohol)

被引：46

作者：

Gandhi, S. ^{[1
]}

Abiramipriya, P. ^{[2
]}

Pooja, N. ^{[2
]}

Jeyakumari, J. Juliat Latha ^{[2
]}

Arasi, A. Yelil ^{[3
]}

Dhanalakshmi, V. ^{[1
]}

Nair, M. R. Gopinathan ^{[4
]}

Anbarasan, R. ^{[1
,5
]}

机构：

[1] Kamaraj Coll Engn & Technol, Dept Polymer Technol, Virudunagar 626001, Tamilnadu, India

[2] VVV Coll Women, Dept Phys, Virudunagar 626001, Tamilnadu, India

[3] Kamaraj Coll Engn & Technol, Dept Phys, Virudunagar 626001, Tamilnadu, India

[4] Mahatma Gandhi Univ, Sch Chem Sci, Kottayam 686560, Keralam, India

[5] Natl Taiwan Univ, MEMS Thermal Control Lab, Dept Mech Engn, Taipei 10617, Taiwan

来源：

JOURNAL OF NON-CRYSTALLINE SOLIDS | 2011年 / 357卷 / 01期

关键词：

One pot method; PVA/MgO nano composite; FTIR; XRD; HRTEM; DSC; TGA; CHEMICAL-VAPOR-DEPOSITION; NANOCRYSTALS; NANOWIRES; NANOTUBES; SURFACE; FILMS;

D O I：

10.1016/j.jnoncrysol.2010.09.050

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Magnesium oxide (MgO) nano particle was synthesized by ultrasound assisted one pot method and thus synthesized nano MgO was mixed with poly(vinyl alcohol) (PVA) to prepare the polymer nano composite. The influence of the nano sized MgO on the structural modification of PVA was evaluated. The particle size and morphology of MgO was confirmed by High Resolution Transmission Electron Microscopy (HRTEM). The properties of PVA/MgO nano composite materials were characterized by Fourier Transform Infrared analysis (FTIR), Thermogravimetric analysis (TGA) and Differential scanning calorimetry (DSC) like analytical tools. (C) 2010 Elsevier B.V. All rights reserved.

引用

页码：181 / 185

页数：5

共 22 条

[1] ESTIMATION ON THERMAL-CONDUCTIVITIES OF FILLED POLYMERS [J].

AGARI, Y ;

UNO, T .

JOURNAL OF APPLIED POLYMER SCIENCE, 1986, 32 (07) :5705-5712

[2] Morphology, surface topography and optical studies on electron beam evaporated MgO thin films [J].

Chowdhury, A. ;

Kumar, J. .

BULLETIN OF MATERIALS SCIENCE, 2006, 29 (05) :513-521

[3] Synthesis of MgO powders from molten salts [J].

Du, YS ;

Inman, D .

JOURNAL OF MATERIALS SCIENCE, 1997, 32 (09) :2373-2379

[4] Combustion synthesis and photoluminescence of MgO:Eu3+ nanocrystals with Li+ addition [J].

Gu, F ;

Li, CZ ;

Jiang, HB .

JOURNAL OF CRYSTAL GROWTH, 2006, 289 (01) :400-404

[5] Chemistry and physics in one dimension: Synthesis and properties of nanowires and nanotubes [J].

Hu, JT ;

Odom, TW ;

Lieber, CM .

ACCOUNTS OF CHEMICAL RESEARCH, 1999, 32 (05) :435-445

[6] Preparation of highly dispersed MgO and its bactericidal properties [J].

Huang, L ;

Li, DQ ;

Evans, DG ;

Duan, X .

EUROPEAN PHYSICAL JOURNAL D, 2005, 34 (1-3) :321-323

[7] Effect of Sm addition on Ni-MgO catalysts for the synthesis of carbon nanotubes via methane decomposition [J].

Li, K ;

Lu, GX ;

Wang, WP ;

Li, JZ ;

Liu, JF .

CHEMISTRY LETTERS, 2005, 34 (01) :48-49

[8] Structure-sensitive biodiesel synthesis over MgO nanocrystals [J].

Montero, Janine M. ;

Gai, Pratibha ;

Wilson, Karen ;

Lee, Adam F. .

GREEN CHEMISTRY, 2009, 11 (02) :265-268

[9] Preparation of MgO films by atmospheric metal-organic chemical vapor deposition as a protective layer in AC plasma display panels [J].

Okada, Takeru ;

Komaki, Toshihiro .

JAPANESE JOURNAL OF APPLIED PHYSICS, 2008, 47 (03) :1699-1705

[10] Synthesis and characterizations of nano-sized Ni(OH)2 and Ni(OH)2/poly(vinyl alcohol) nano composite [J].

Parveen, M. Fathima ;

Umapathy, S. ;

Dhanalakshmi, V. ;

Anbarasan, R. .

JOURNAL OF MATERIALS SCIENCE, 2009, 44 (21) :5852-5860

← 1 2 3 →