Preparation and magnetic properties of ZnFe2O4 nanofibers by coprecipitation-air oxidation method

被引：36

作者：

Li, Qiaoling ^{[1
]}

Bo, Changchuan ^{[1
]}

Wang, Wenting ^{[1
]}

机构：

[1] N Univ China, Sch Sci, Dept Chem, Taiyuan 030051, Peoples R China

来源：

MATERIALS CHEMISTRY AND PHYSICS | 2010年 / 124卷 / 2-3期

关键词：

ZnFe2O4; nanofibers; Coprecipitation-air oxidation method; Magnetic properties; X ray diffraction; FABRICATION; MANGANESE; NANORODS; GROWTH; NICKEL;

D O I：

10.1016/j.matchemphys.2010.07.058

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

ZnFe2O4 nanofibers have been reproducibly synthesized by the thermal treatment of the fiber-like precursor that was fabricated by the oxidation of a coprecipitation product obtained by Zn2+ and Fe2+ in a NaOH solution The phase morphology and particle diameter were examined by X-ray diffraction (XRD) and transmission electron microscopy (TEM) respectively The magnetic properties of the samples were studied using a vibrating sample magnetometer (VSM) It indicated that the diameters of obtained ZnFe2O4 nanofibers were found to range between 10 and 15 nm the length ranged between 2 and 3 mu m With the increase in the calcination temperature the length of ZnFe2O4 nanofibers reduced and the diameter increased appreciably the coerciviy of the ZnFe2O4 samples reduced and the saturation magnetization increased When the calcination temperature was 600 C the coercivity saturation magnetization and remanent magnetization of the samples were 931 Oe 23 5 emu g(-1) and 4 3 emu g-1 respectively evidently far higher than those of the spherical ZnFe2O4 (c) 2010 Elsevier B V All rights reserved

引用

页码：891 / 893

页数：3

共 25 条

[1] ZnFe2O4 nanoparticles: Microwave-hydrothermal ionic liquid synthesis and photocatalytic property over phenol [J].

Cao, Shao-Wen ;

Zhu, Ying-Jie ;

Cheng, Guo-Feng ;

Huang, Yue-Hong .

JOURNAL OF HAZARDOUS MATERIALS, 2009, 171 (1-3) :431-435

[2] Atomic structure and magnetic properties of MnFe2O4 nanoparticles produced by reverse micelle synthesis [J].

Carpenter, EE ;

O'Connor, CJ ;

Harris, VG .

JOURNAL OF APPLIED PHYSICS, 1999, 85 (08) :5175-5177

[3]

CHE AX, 1997, CHEM WORLD, V4, P404

[4]

CHE AX, 1999, J CHEM PHYS, V2, P211

[5] Growth of nanowire superlattice structures for nanoscale photonics and electronics [J].

Gudiksen, MS ;

Lauhon, LJ ;

Wang, J ;

Smith, DC ;

Lieber, CM .

NATURE, 2002, 415 (6872) :617-620

[6] Lithium storage in hollow spherical ZnFe2O4 as anode materials for lithium ion batteries [J].

Guo, Xianwei ;

Lu, Xia ;

Fang, Xiangpeng ;

Mao, Ya ;

Wang, Zhaoxiang ;

Chen, Liquan ;

Xu, Xiaoxue ;

Yang, Hong ;

Liu, Yinong .

ELECTROCHEMISTRY COMMUNICATIONS, 2010, 12 (06) :847-850

[7]

HUANG Y, 2001, LIEBER SCI, V29, P630

[8] Influence of manganese on iron oxyhydroxides and oxides formed in aqueous solution [J].

Inoue, Katsuya ;

Okui, Masato ;

Tanaka, Masahiko ;

Shinoda, Kozo ;

Suzuki, Shigeru ;

Waseda, Yoshio .

CORROSION SCIENCE, 2008, 50 (03) :811-817

[9] Surface spin disorder in NiFe2O4 nanoparticles [J].

Kodama, RH ;

Berkowitz, AE ;

McNiff, EJ ;

Foner, S .

PHYSICAL REVIEW LETTERS, 1996, 77 (02) :394-397

[10] Synthesis and characterization of ZnFe2O4 magnetic nanoparticles via a PEG-assisted route [J].

Koseoglu, Yuksel ;

Baykal, Abduelhadi ;

Toprak, Muhammet S. ;

Gozuak, Fatma ;

Basaran, Ali Cemil ;

Aktas, Bekir .

JOURNAL OF ALLOYS AND COMPOUNDS, 2008, 462 (1-2) :209-213

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