NQR Study of AlBr3 Complexes with Dimethylsulfide

被引：0

作者：

Ishihara, Hideta ^{[1
]}

Sirahama, Tomoaki ^{[1
]}

Nakashima, Shouko ^{[1
]}

Terao, Hiromitsu ^{[2
]}

Yamada, Koji ^{[3
]}

机构：

[1] Saga Univ, Fac Culture & Educ, Saga 8408502, Japan

[2] Univ Tokushima, Fac Integrated Arts & Sci, Tokushima 7708502, Japan

[3] Nihon Univ, Coll Ind Technol, Chiba 2758576, Japan

来源：

ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES | 2011年 / 66卷 / 05期

关键词：

Br-81 and Al-27 NQR; Polymorphism; AlBr3 Complexes with (CH3)(2)S; NUCLEAR-QUADRUPOLE RESONANCE;

D O I：

10.5560/ZNB.2011.66b0541

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Br-81-Al-27 SEDOR as well as Br-81 NQR spectroscopy have been applied to the molecular complexes of AlBr3 with (CH3)(2)S. The formation of two kinds of complex compounds, [(CH3)(2)S](2)AlBr3 and [(CH3)(2)S]AlBr3, has been recognized. The compound [(CH3)(2)S](2)AlBr3 is a solid at ambient temperature, while the compound [(CH3)(2)S]AlBr3 is a liquid with a melting point of 287 K. The crystalline state of [(CH3)(2)S]AlBr3 shows a complex polymorphism consisting of Forms 1, 2 and 3 in which conformation isomers of [(CH3)(2)S]AlBr3 seem to exist. The structures of the complex compounds are discussed together with the results of ab initio MO calculations.

引用

页码：541 / 544

页数：4

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