Crystal structure of 3,3-dihydroxymethyl-1,6-dioxa-spiro[5.5]undecane, C11H20O4

被引：6

作者：

Yuan, Lin ^{[1
]}

Shi, Jiang-Hua ^{[1
]}

Zhang, Min ^{[1
]}

机构：

[1] Hunan Univ Sci & Engn, Dept Biol & Chem, Yongzhou 425100, Hunan, Peoples R China

来源：

ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2012年 / 227卷 / 01期

关键词：

CLEAVABLE SURFACTANTS; 1,3-DIOXANE RING;

D O I：

10.1524/ncrs.2012.0016

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

C11H20O4, triclinic, P (1) over bar (no. 2), a = 6.014(2) angstrom, b = 9.566(3) angstrom, c = 10.135(4) angstrom, alpha = 96.669(6)degrees, beta = 94.985(6)degrees, gamma = 97.419(6)degrees, V = 571.2 angstrom(3), Z = 2, R-gt(F) = 0.053, wR(ref)(F-2) = 0.179, T = 298 K.

引用

页码：35 / 36

页数：2

共 6 条

[1] THE CHEMICAL REACTIONS OF PENTAERYTHRITOL AND ITS DERIVATIVES [J].

MARRIAN, SF .

CHEMICAL REVIEWS, 1948, 43 (01) :149-202

[2] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[3] PREPARATION AND PROPERTIES OF SULFONATE SALT-TYPE CLEAVABLE SURFACTANTS WITH A 1,3-DIOXANE RING [J].

WANG, GW ;

YUAN, XY ;

LIU, YC ;

LEI, XG .

JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1994, 71 (07) :727-730

[4] (5-n-Heptyl-2-hydroxymethyl-1,3-dioxan-2-yl)methanol [J].

Yuan, Xian-You ;

Zhang, Min ;

Ng, Seik Weng .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O2918-U1081

[5]

Yuan XY, 2005, CHINESE J ORG CHEM, V25, P1049

[6] (5-n-Hexyl-2-hydroxymethyl-1,3-dioxan2-yl)methanol [J].

Zhang, Min ;

Yuan, Xian-You ;

Ng, Seik Weng .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O2917-U1069

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