Measurement and Correlation for the Solubility of Dimethyl 1,4-Cyclohexanedione-2,5-dicarboxylate in Different Solvents at Temperatures from (278.15 to 323.15) K

被引:26
作者
Chen, Zhao-guo [1 ]
Yang, Wen-ge [1 ]
Hu, Yong-Hong [1 ]
Lei, Zi-Yu [1 ]
Wang, Yao-Han [1 ]
Wan, Wen-Qian [1 ]
机构
[1] Nanjing Univ Technol, Coll Biotechnol & Pharmaceut Engn, Nanjing 210009, Peoples R China
关键词
ETHANOL; METHANOL; WATER;
D O I
10.1021/je2000292
中图分类号
O414.1 [热力学];
学科分类号
摘要
As an urgent need in the design and upscale of the industrial crystallization process, on the basis of the isothermal saturated method, the solubility of dimethyl 1,4-cyclohexanedione-2,5-dicarboxylate in N,N-dimethylformamide, methanol, I-propanol, acetonitrile, 2-propanol, ethyl acetate, and acetone was measured at atmospheric pressure. The experimental data were well-correlated with the lambda h model. The calculated solubilities show good agreement with the experimental solubility data. To our knowledge, this is the first time the solubilities of dimethyl 1,4-cyclohexanedione-2,5-dicarboxylate are reported.
引用
收藏
页码:2726 / 2729
页数:4
相关论文
共 20 条
[1]   SOLUBILITY OF TRIOXANE IN WATER [J].
BRANDANI, S ;
BRANDANI, V ;
FLAMMINI, D .
JOURNAL OF CHEMICAL AND ENGINEERING DATA, 1994, 39 (02) :201-202
[2]  
CAMPBELL CD, 1993, EP536083
[3]   SCREENING OF SUITABLE SOLVENTS IN ORGANIC-SYNTHESIS - STRATEGIES FOR SOLVENT SELECTION [J].
CARLSON, R ;
LUNDSTEDT, T ;
ALBANO, C .
ACTA CHEMICA SCANDINAVICA SERIES B-ORGANIC CHEMISTRY AND BIOCHEMISTRY, 1985, 39 (02) :79-91
[4]   Solubility and Crystal Size of Sirolimus in Different Organic Solvents [J].
Gandhi, Pankaj J. ;
Murthy, Z. V. P. .
JOURNAL OF CHEMICAL AND ENGINEERING DATA, 2010, 55 (11) :5050-5054
[5]   Measurement and Correlation of Griseofulvin Solubility in Different Solvents at Temperatures from (281.95 to 357.60) K [J].
Hu, Guoqin ;
Li, Hua ;
Wang, Xiaojun ;
Zhang, Yadong .
JOURNAL OF CHEMICAL AND ENGINEERING DATA, 2010, 55 (09) :3969-3971
[6]   Solubility of sodium dimethyl isophthalate-5-sulfonate in water and in water plus methanol containing sodium sulfate [J].
Jiang, Q ;
Gao, GH ;
Yu, YX ;
Qin, Y .
JOURNAL OF CHEMICAL AND ENGINEERING DATA, 2000, 45 (02) :292-294
[7]   Muscarinic acetylcholine receptor antagonists: SAR and optimization of tyrosine ureas [J].
Jin, Jian ;
Wang, Yonghui ;
Shi, Dongchuan ;
Wang, Feng ;
Fu, Wei ;
Davis, Roderick S. ;
Jin, Qi ;
Foley, James J. ;
Sarau, Henry M. ;
Morrow, Dwight M. ;
Moore, Michael L. ;
Rivero, Ralph A. ;
Palovich, Michael ;
Salmon, Michael ;
Belmonte, Kristen E. ;
Busch-Petersen, Jakob .
BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2008, 18 (20) :5481-5486
[8]   Solubility of potassium dichromate in dilute aqueous ethanol solutions in the temperature range 283 K to 303 K [J].
Korin, E ;
Soifer, L .
JOURNAL OF CHEMICAL AND ENGINEERING DATA, 1997, 42 (06) :1251-1253
[9]   Measurement and Correlation of Solubility of Pimelic Acid in Ether, Tetrahydrofuran, Ethanol, and Methanol [J].
Li, Hua ;
Zhu, Jiang ;
Hu, Guoqin ;
Jiang, Pinliang ;
Zhao, Lei ;
Zhang, Yadong .
JOURNAL OF CHEMICAL AND ENGINEERING DATA, 2010, 55 (03) :1443-1445
[10]   Synthesis and Properties of Poly[p-(2,5-dihydroxy)-phenylenebenzobisoxazole] Fiber [J].
Lin, Hong ;
Huang, Yu-Dong ;
Wang, Feng .
INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES, 2008, 9 (11) :2159-2168