Polysiloxane-encapsulated stationary phase for reversed-phase high-performance liquid chromatography

被引：5

作者：

Jiang, SX ^{[1
]}

Yang, RQ ^{[1
]}

Chen, LR ^{[1
]}

机构：

[1] CHINESE ACAD SCI,LANZHOU INST CHEM PHYS,DIV ANALYT CHEM,LANZHOU 730000,PEOPLES R CHINA

来源：

CHROMATOGRAPHIA | 1997年 / 44卷 / 5-6期

关键词：

column liquid chromatography; encapsulated stationary phase; poly(methylvinylsiloxane);

D O I：

10.1007/BF02466392

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Silica beads of 6-mu m average diameter were silanized with methylvinyldiethoxysilane and then subjected to encapsulation with poly(methylvinylsiloxane). The resulting product is a new stationary phase for reversed-phase high performance liquid chromatography (RP-HPLC) which has superior ability for the separation of polar, non-polar and basic compounds. The chromatographic peaks are symmetric. Its stability has been studied; after continuous use for three months the carbon content and chromatographic behaviour of the phase were unchanged.

引用

页码：263 / 266

页数：4

共 6 条

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