Syntheses of new (CdO)(1-X)(NiO)XZnO nanocomposite system: Preparation, structure, and magnetic properties

被引:10
作者
Afify, Nasser [1 ]
机构
[1] Assiut Univ, Dept Phys, Fac Sci, Assiut 71516, Egypt
来源
MATERIALS SCIENCE AND ENGINEERING B-ADVANCED FUNCTIONAL SOLID-STATE MATERIALS | 2021年 / 273卷
关键词
Cadmium Nickel Zinc Oxide nanocomposite; Crystal structure; SEM and HRTEM micrographs; FTIR; Magnetic properties and hydrothermal reaction; CDO-ZNO NANOCOMPOSITE; NICKEL-OXIDE; NIO; NANOPARTICLES; CO; COMPOSITE;
D O I
10.1016/j.mseb.2021.115399
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
This paper presents a new nanocomposite system of (CdO)((1-X))(NiO)(X)ZnO (0 <= Chi <= 1 mol). The proposed nanocomposite system is synthesized using a hydrothermal method to experimentally study the structure and magnetic properties of the (CdO)((1-X))(NiO)(X)ZnO (0 <= Chi <= 1 mol) system. The formations of the nanocomposite with CdO (face-centered cubic) and ZnO (hexagonal) phases are determined using the X-ray diffraction analysis (XRD) diffractogram and they are confirmed with a high-resolution transmission electron microscope (HRTEM). In our study, we use a Celref Unit-Cell refinement code to determine the crystallization parameters, lattice parameter (a, b and c), bond length (Iota), cell volume (nu) and theoretical density (rho), while the average crystallite size (D-av), dislocation density (delta), and the microstrain (c) are determined using the Scherrer equation. Additionally, we analyze the magnetization curves and the mass magnetic susceptibility (chi(mass)) of the nanocomposites (CdO)((1-X))(NiO)(X)ZnO system using a Vibrating Sample Magnetometer (VSM). Lastly, the effect of substituting Cd+2 ions by Ni+2 ions on the above properties is discussed.
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页数:8
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