Neutron spin echo scattering angle measurement (SESAME)

被引:24
作者
Pynn, R
Fitzsimmons, MR
Fritzsche, H
Gierlings, M
Major, J
Jason, A
机构
[1] Los Alamos Natl Lab, Los Alamos, NM 87545 USA
[2] Natl Res Council Canada, Chalk River Labs, SIMS, Chalk River, ON K0J 1P0, Canada
[3] Hahn Meitner Inst Berlin GmbH, D-14109 Berlin, Germany
[4] Max Planck Inst Met Res, D-70569 Stuttgart, Germany
关键词
D O I
10.1063/1.1884187
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
We describe experiments in which the neutron spin echo technique is used to measure neutron scattering angles. We have implemented the technique, dubbed spin echo scattering angle measurement (SESAME), using thin films of Permalloy electrodeposited on silicon wafers as sources of the magnetic fields within which neutron spins precess. With 30-μ m-thick films we resolve neutron scattering angles to about 0.02° with neutrons of 4.66 A wavelength. This allows us to probe correlation lengths up to 200 nm in an application to small angle neutron scattering. We also demonstrate that SESAME can be used to separate specular and diffuse neutron reflection from surfaces at grazing incidence. In both of these cases, SESAME can make measurements at higher neutron intensity than is available with conventional methods because the angular resolution achieved is independent of the divergence of the neutron beam. Finally, we discuss the conditions under which SESAME might be used to probe in-plane structure in thin films and show that the method has advantages for incident neutron angles close to the critical angle because multiple scattering is automatically accounted for. © 2005 American Institute of Physics.
引用
收藏
页数:15
相关论文
共 50 条
[31]   Probing magnetic correlations with spin-echo modulated small angle neutron scattering (SEMSANS) [J].
Li, Fankang ;
Steinke, Nina J. ;
Dalgliesh, Robert M. ;
Washington, Adam L. ;
Shen, Jiazhou ;
Pynn, Roger ;
Parnell, Steven R. .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2021, 1014
[32]   Elucidation of spin echo small angle neutron scattering correlation functions through model studies [J].
Shew, Chwen-Yang ;
Chen, Wei-Ren .
JOURNAL OF CHEMICAL PHYSICS, 2012, 136 (06)
[33]   Increased solid angle in neutron resonance spin echo [J].
Haeussler, W. ;
Schmidt, U. ;
Dubbers, D. .
PHYSICA B-CONDENSED MATTER, 2004, 350 (1-3) :E799-E802
[34]   Construction of a Spin-Echo Small-Angle Neutron Scattering Instrument for the PIK Reactor [J].
Chetverikov, Yu. O. ;
Akselrod, L. A. ;
Grigor'ev, S. V. ;
Kraan, V. ;
Sumbatyan, A. A. ;
Nagorny, A. V. ;
Tarnavich, V. V. .
JOURNAL OF SURFACE INVESTIGATION, 2022, 16 (05) :831-838
[35]   The use of symmetry to correct Larmor phase aberrations in spin echo scattering angle measurement [J].
Pynn, Roger ;
Lee, W. T. ;
Stonaha, P. ;
Shah, V. R. ;
Washington, A. L. ;
Kirby, B. J. ;
Majkrzak, C. F. ;
Maranville, B. B. .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2008, 79 (06)
[36]   Spin echo small-angle neutron scattering using superconducting magnetic Wollaston prisms [J].
Funama, Fumiaki ;
Wolf, Caitlyn M. ;
Weigandt, Katie ;
Shen, Jiazhou ;
Parnell, Steven R. ;
Li, Fankang .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2024, 95 (07)
[37]   Porosity of silica Stober particles determined by spin-echo small angle neutron scattering [J].
Parnell, S. R. ;
Washington, A. L. ;
Parnell, A. J. ;
Walsh, A. ;
Dalgliesh, R. M. ;
Li, F. ;
Hamilton, W. A. ;
Prevost, S. ;
Fairclough, J. P. A. ;
Pynn, R. .
SOFT MATTER, 2016, 12 (21) :4709-4714
[38]   Magnetic design of a spin-echo small-angle neutron-scattering instrument [J].
Uca, O ;
Bouwman, WG ;
Rekveldt, MT .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2003, 496 (2-3) :437-445
[39]   Spin echo small angle neutron scattering using a continuously pumped 3He neutron polarisation analyser [J].
Parnell, S. R. ;
Washington, A. L. ;
Li, K. ;
Yan, H. ;
Stonaha, P. ;
Li, F. ;
Wang, T. ;
Walsh, A. ;
Chen, W. C. ;
Parnell, A. J. ;
Fairclough, J. P. A. ;
Baxter, D. V. ;
Snow, W. M. ;
Pynn, R. .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2015, 86 (02)
[40]   Present status and prospects for Spin-Echo Small-Angle Neutron Scattering (SESANS) at PIK neutron source [J].
Kraan W.H. ;
Akselrod L.A. ;
Chetverikov Y.O. ;
Grigoriev S.V. ;
Moskwin E.V. ;
Piyadov V.V. ;
Set K.T. ;
Sumbatyan A.A. ;
Velichko E.V. ;
Zabenkin V.N. .
Kraan, W.H., 1600, Izdatel'stvo Nauka (08) :1035-1043