Microwave-Assisted Synthesis of N-Monosubstituted Urea Derivatives

被引：15
|
作者：
De Luca, Lidia [1 ]
Porcheddu, Andrea [1 ]
Giacomelli, Giampaolo [1 ]
Murgia, Irene [1 ]
机构：
[1] Univ Sassari, Dipartimento Chim, I-07100 Sassari, Italy
来源：
SYNLETT | 2010年 / 16期
关键词：
urea; potassium cyanate; microwave; N-carbamoyl derivatives; CYANIC ACID; CARBON-MONOXIDE; PRIMARY AMINES; CARBONYLATION; KINETICS; INHIBITORS; CONVERSION; CATALYSIS; CLOSURE; SULFUR;
D O I：
10.1055/s-0030-1258553
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
An easy and rapid procedure for the preparation of N-monosubstituted ureas via reaction between potassium cyanate and a wide range of amines is described. The procedure was performed under microwave irradiation using water as solvent. This methodology is particularly attractive since it provides ureas in high yield and purity.
引用
收藏
页码：2439 / 2442
页数：4
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